2. AOACRIChemContMethods-2018Awards

M astovska et al .: J ournal of AOAC I nternational V ol . 98, N o . 2, 2015  497

Table 7. Collaborative study results (in µg/kg) obtained by the participating laboratories in blind duplicates fortified at the mid PAH level in mussel Laboratory No. PAH Sample ID 1 2 3 4 5 6 7 8 9 10 1,7-DMP SFC M3 5.7 a 48.0 45.9 27.4 46.1 40.5 42.9 43.8 28.2 36.6 SFC M5 39.0 a 38.5 41.7 31.0 44.1 38.9 42.1 57.2 28.8 28.1 1-MN SFC M3 79.1 92.7 136.2 97.2 95.5 90.3 105.4 110.0 103.5 72.1 SFC M5 78.2 105.0 117.3 87.2 97.2 103.0 109.8 119.5 87.4 50.7 1-MP SFC M3 60.2 a 55.2 54.3 32.2 52.2 47.1 50.6 50.5 31.5 50.9 SFC M5 870.8 a 41.7 48.0 30.1 49.1 44.9 51.0 63.2 31.7 40.3 2,6-DMN SFC M3 21.5 a 64.6 69.5 92.3 79.9 63.1 57.6 62.3 43.0 71.7 a SFC M5 59.2 a 63.6 62.1 85.7 74.9 59.4 61.7 64.0 43.3 92.5 a 3-MC SFC M3 70.3 81.5 101.6 80.7 93.8 93.4 93.3 91.4 78.6 98.9 SFC M5 69.8 86.6 95.8 70.4 87.4 90.3 95.4 97.3 69.5 96.9 Ant SFC M3 22.5 17.5 16.5 7.1 8.2 16.5 14.5 13.8 12.3 13.5 SFC M5 14.9 13.6 14.4 11.0 6.6 13.7 14.8 15.2 10.8 14.7 BaA SFC M3 22.3 21.0 24.8 18.4 21.5 23.2 22.7 22.3 19.6 23.9 SFC M5 22.2 21.3 23.1 16.3 18.8 21.7 23.3 22.3 17.1 23.5 BaP SFC M3 7.4 9.1 10.0 6.6 6.8 1.1 b 9.2 9.8 7.7 8.4 SFC M5 7.6 8.5 8.8 5.6 5.9 1.1 b 9.4 9.9 6.4 7.8 BbF SFC M3 28.2 27.3 29.2 24.0 28.9 31.6 27.9 27.6 24.3 29.9 SFC M5 28.3 27.3 27.1 21.0 26.9 25.0 28.4 26.9 21.3 29.8 BghiP SFC M3 8.8 9.1 10.8 8.1 9.5 9.8 10.0 9.7 7.5 11.0 SFC M5 9.5 9.0 9.8 7.1 8.9 9.3 10.1 9.3 7.3 10.8 BkF SFC M3 18.7 18.1 22.0 15.2 19.5 21.0 19.3 19.2 16.1 21.9 SFC M5 18.8 18.3 20.0 14.0 18.2 17.2 19.0 18.9 13.9 21.4 Chr SFC M3 92.7 86.1 100.8 79.7 98.0 95.2 93.2 92.0 86.0 105.2 SFC M5 94.5 91.3 94.0 70.8 91.4 91.7 94.9 95.5 76.0 102.0 DBahA SFC M3 8.8 9.4 9.7 8.0 9.4 9.9 9.6 9.5 6.3 11.0 SFC M5 8.5 9.2 8.9 7.1 8.8 8.9 10.0 9.5 7.5 11.2 Fln SFC M3 24.8 25.0 26.8 29.2 25.2 24.9 24.5 24.5 23.9 28.5 SFC M5 24.3 25.6 25.1 29.6 23.6 24.1 25.1 26.0 21.9 26.5 Flt SFC M3 47.8 45.5 49.7 46.6 50.8 55.3 48.1 48.2 39.2 55.6 SFC M5 53.7 47.6 46.8 42.1 47.2 54.5 49.0 49.5 46.6 53.3 IcdP SFC M3 9.0 9.6 10.1 8.1 9.7 10.1 9.5 9.7 8.6 11.3 SFC M5 9.5 9.3 9.8 7.2 9.1 9.2 9.9 9.5 6.9 11.4 Naph SFC M3 91.8 125.4 134.8 84.0 104.1 97.1 124.2 129.6 123.9 71.7 SFC M5 84.6 122.2 127.8 65.1 107.7 114.8 124.8 135.3 109.7 40.0 Phe SFC M3 92.1 206.3 b 102.0 81.9 102.1 93.7 95.1 94.3 a 84.3 98.8 SFC M5 97.1 191.3 b 93.9 76.3 96.2 90.5 96.6 119.2 a 82.5 107.0 Pyr SFC M3 79.2 71.9 80.3 62.0 75.6 71.2 72.4 72.2 64.2 80.2 SFC M5 75.4 74.6 75.8 55.5 70.4 69.3 73.3 72.0 58.2 76.7

a  Outliers removed by the Cochran test. b Outliers removed by single Grubbs’ test.