2. AOACRIChemContMethods-2018Awards

498  M astovska et al . : J ournal of AOAC I nternational V ol . 98, N o . 2, 2015

Table 8. Collaborative study results (in µg/kg) obtained by the participating laboratories in blind duplicates fortified at the high PAH level in mussel Laboratory No. PAH Sample ID 1 2 3 4 5 6 7 8 9 10 1,7-DMP SFC M2 34.5 39.8 41.4 26.1 44.7 40.4 46.8 43.6 30.2 37.6 SFC M7 22.4 34.0 42.2 26.5 47.0 39.3 48.5 56.7 30.7 45.8 1-MN SFC M2 183.7 222.9 a 211.8 199.1 193.9 195.7 196.9 190.0 206.8 387.8 b SFC M7 274.7 459.3 a 218.8 241.5 198.7 208.8 199.6 220.5 199.4 62.0 b 1-MP SFC M2 431.7 b 113.4 122.8 81.6 128.5 115.8 135.8 123.1 79.6 125.9 SFC M7 1752.2 b 102.7 129.2 81.9 133.2 112.6 137.7 146.5 79.7 159.3 2,6-DMN SFC M2 139.5 128.0 138.5 214.2 177.8 143.4 142.1 161.2 98.7 184.6 SFC M7 121.6 135.2 158.1 244.0 187.9 141.7 149.4 144.7 94.2 171.3 3-MC SFC M2 100.6 133.6 147.7 127.2 146.5 146.7 150.4 138.0 127.4 149.4 SFC M7 103.5 130.3 156.7 128.4 151.9 144.9 151.9 145.6 121.6 157.7 Ant SFC M2 35.3 44.7 b 39.9 19.9 20.9 37.7 37.1 33.2 31.2 29.0 SFC M7 31.7 33.9 b 42.8 16.3 20.3 38.9 37.5 33.7 31.7 29.9 BaA SFC M2 51.1 49.3 52.2 43.4 b 49.9 53.3 54.9 50.0 47.7 a 54.1 SFC M7 52.0 50.7 55.0 41.7 b 51.2 52.9 55.8 53.3 476.3 b 56.1 BaP SFC M2 19.1 19.8 22.3 15.6 16.6 3.0 a 22.4 22.4 19.8 17.6 SFC M7 18.3 19.4 22.9 15.1 17.0 3.0 a 22.6 20.8 18.5 17.5 BbF SFC M2 74.8 68.2 65.5 59.0 71.1 74.8 70.4 66.6 62.7 71.9 SFC M7 71.8 67.2 68.5 58.8 74.1 77.2 71.2 69.5 60.3 78.1 BghiP SFC M2 18.2 18.0 18.2 15.1 17.9 18.3 18.9 17.4 16.3 19.5 SFC M7 18.8 17.6 19.7 14.9 18.7 18.0 19.3 18.4 15.2 20.3 BkF SFC M2 38.8 33.8 38.8 30.8 37.3 36.3 38.3 36.9 30.5 41.7 SFC M7 37.9 35.0 37.8 30.6 37.9 39.5 38.2 37.7 30.4 43.8 Chr SFC M2 159.8 158.5 153.2 137.7 166.6 163.9 164.1 152.1 150.9 174.8 SFC M7 166.8 152.4 165.9 139.2 172.3 161.0 165.6 161.0 145.3 184.1 DBahA SFC M2 13.7 13.7 13.6 12.1 13.7 13.3 14.8 13.2 13.2 15.0 SFC M7 13.9 13.0 14.5 10.6 14.3 13.2 14.8 14.0 12.3 15.4 Fln SFC M2 50.2 49.0 45.8 59.2 a 47.5 47.0 47.3 46.0 49.4 50.7 SFC M7 49.8 49.1 49.8 59.4 a 48.0 46.6 48.4 43.0 45.1 53.0 Flt SFC M2 92.6 88.7 86.7 66.5 a 96.2 96.5 93.4 89.7 93.1 100.2 SFC M7 104.7 88.4 93.6 63.4 a 98.1 93.7 94.7 84.1 79.6 104.3 IcdP SFC M2 17.8 18.3 17.2 15.5 18.7 18.6 18.4 17.3 16.7 19.0 SFC M7 17.0 16.6 18.7 15.3 19.7 19.3 18.5 18.3 15.2 21.3 Naph SFC M2 125.2 b 149.8 143.7 108.7 134.0 138.5 159.5 165.5 164.9 246.4 b SFC M7 197.9 b 160.7 160.0 104.6 141.0 144.4 159.0 165.6 146.5 34.3 b Phe SFC M2 159.7 452.2 b 159.4 142.5 173.2 161.0 166.2 162.4 143.6 164.0 b SFC M7 178.0 366.3 b 170.3 142.9 177.6 159.0 169.8 167.6 139.0 200.9 b Pyr SFC M2 133.5 119.2 114.3 102.2 119.8 114.8 118.6 108.3 104.4 124.3 SFC M7 123.0 117.5 122.6 102.9 125.1 113.3 120.1 119.2 97.4 128.6

a Outliers removed by the Cochran test. b Outliers removed by single Grubbs’ test.