2015.14 Vitamin B (July 2018)

2015.14 (JULY 2018) BVit-02 AOAC_Riboflavin_Tot_MLT- AOAC_BlindDup_00859RF00

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AOAC International Interlaboratory Study Workbook

Version:

2.1

Blind (Unpaired) Replicates Calculations Sheet

AOAC 2015.14 Simultaneous Determination of Total Vitamins B1, B2, B3, and B6 in Infant Formula and Related Nutritiona

Summary Statistics

0.0552 Largest within variance 2.0870 Largest average lab result 1.6045 Smallest average lab result 1.9150 Grand average of all lab averages

0.13119 S(2H)

2.0870 Max Val(1) 2.0700 Max Val(2) 1.6045 Min Val(1) 1.8029 Min Val(2) 0.0919 S(HL) 2.0870 Max Val 1.6045 Min Val 0.0896 S(2L)

0.14433 s

0.13901 S(h) 0.10023 S(l)

2.087 1.6045

10 # Laboratories

Average Lab Result^2

Average Lab Result^2 Results^2

Average Lab Result

Sum of Lab Results

# Lab Replicates given

Sum of Results^2/#Reps DEVN of Sq

Variance within DEVN of Sq

Lab

1 2 3 4 5 6 7 8 9

2 3.8000 1.9000 2 3.2090 1.6045 2 4.1740 2.0870 2 4.1400 2.0700 2 4.1000 2.0500 2 3.7897 1.8949 2 3.6057 1.8029 2 3.9300 1.9650 2 3.7116 1.8558 2 3.8395 1.9198

3.6100 2.5744 4.3556 4.2849 4.2025 3.5905 3.2504 3.8612 3.4441 3.6855

7.2218 5.1523 8.7116 8.6068 8.4052 7.1882 6.5013 7.7294 6.8885 7.4262

7.2200 5.1488 8.7111 8.5698 8.4050 7.1809 6.5007 7.7225 6.8881 7.3710

0.0018 0.0018 0.0034 0.0034 0.0005 0.0005 0.0370 0.0370 0.0002 0.0002 0.0073 0.0073 0.0006 0.0006 0.0069 0.0069 0.0004 0.0004 0.0552 0.0552

0.0018 Lab 1 0.0034 Lab 2 0.0005 Lab 3 0.0370 Lab 4 0.0002 Lab 5 0.0073 Lab 6 0.0006 Lab 7 0.0069 Lab 8 0.0004 Lab 9 0.0552 Lab 10

1.9000 Lab 1 1.6045 Lab 2 2.0870 Lab 3 2.0700 Lab 4 2.0500 Lab 5 1.8949 Lab 6 1.8029 Lab 7 1.9650 Lab 8 1.8558 Lab 9 1.9198 Lab 10

10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49

Lab 11 Lab 12 Lab 13 Lab 14 Lab 15 Lab 16 Lab 17 Lab 18 Lab 19 Lab 20 Lab 21 Lab 22 Lab 23 Lab 24 Lab 25 Lab 26 Lab 27 Lab 28 Lab 29 Lab 30 Lab 31 Lab 32 Lab 33 Lab 34 Lab 35 Lab 36 Lab 37 Lab 38 Lab 39 Lab 40 Lab 41 Lab 42 Lab 43 Lab 44 Lab 45 Lab 46 Lab 47 Lab 48 Lab 49

Lab 11 Lab 12 Lab 13 Lab 14 Lab 15 Lab 16 Lab 17 Lab 18 Lab 19 Lab 20 Lab 21 Lab 22 Lab 23 Lab 24 Lab 25 Lab 26 Lab 27 Lab 28 Lab 29 Lab 30 Lab 31 Lab 32 Lab 33 Lab 34 Lab 35 Lab 36 Lab 37 Lab 38 Lab 39 Lab 40 Lab 41 Lab 42 Lab 43 Lab 44 Lab 45 Lab 46 Lab 47 Lab 48 Lab 49