2019 Vet Drug Residues ERP - Review Book

AOAC SMPR ERPs - 2019 METHOD REVIEW FORM

Submission Date

2019-09-05 02:09:13

Name

sudhakar yadlaplli

E-mail

sudhakar@firstsourcels.com

Organization

First source laboratory solutions LLP

Title of Method

Veternary Drugs in Food by LCMSMS

AOAC Candidate Method Number (e.g. ALN-01)

VD4S154

Applicable SMPR

AOAC SMPR 2018-010

I. Summary of the Method

The method used for Screen and confirm 154 selected veterinary drug residues in various food matrices including milk based ingredients and products( skimmed milk powder, whey protein, fat filled milk powder, lactose, casein, Infant formula, Infant cereals and baby foods)as well as meat and fish based ingredients and products by using LCMSMS. Yes, covered all milk based products (Milk fractions, Infant formula, Growing up formula, Adult formula, infant cereals and baby foods) and meat and fish based products (fresh, powdered, cooked and baby foods)

II. Review of the Method Only 1. Does the applicability of the method support the applicability of the SMPR? If not, please explain what is missing. 2. Does the analytical technique(s) used in the method meet the SMPR? If not, please specify how it differs from what is stated in the SMPR. 3. Are the definitions specified in the SMPR used and applied appropriately in the method? If no, please indicate how the terms are used. 4. Does the method, as written, contain all appropriate precautions and warnings related to the method's reagents, components, instrumentation, or method steps that may be hazardous? If no, please suggest wording or option(s).

Yes, equipment used was highly sensitive and selective advanced LC-MS/MS (5500 q-trap) which can meet SMPR requirement.

Yes, well defined.

Yes,