6. AOACSPIFANMethods-2018Awards

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1132  Mottier et al. : J ournal of AOAC I nternational Vol. 98, No. 4, 2015

77 → 33

Infant Formula Soya-based LIMS 890000008560 Unspiked

77 → 57

79 → 34 (Internal Std)

79 → 59 (Internal Std)

77 → 33

Infant Formula Soya-based LIMS 890000008560 Spiked at 1 µg/kg

77 → 57

79 → 34 (Internal Std)

79 → 59 (Internal Std)

Figure 2015.03D. LC-MS/MS chromatograms of a powdered soya-based infant formula unspiked and spiked at the 1 µg/kg (IS 10 µg/kg) level. Enclosure 3 – LC-MS/MS chromatograms of a powdered soya-based infant formula unspiked and spiked at the 1 µg/kg (IS 10 µg/kg) level

77 → 33

77 → 57

Milk Infant Formula LIMS 890000008562 Unspiked

79 → 34 (Internal Std)

79 → 59 (Internal Std)

77 → 33

Milk Infant Formula LIMS 890000008562 Spiked at 1 µg/kg

77 → 57

79 → 34 (Internal Std)

79 → 59 (Internal Std)

Figure 2015.03E. LC-MS/MS chromatograms of a powdered milk infant formula unspiked and spiked at the 1 µg/kg (IS 10 µg/kg) level. Enclosure 4 – LC-MS/MS chromatograms of a powdered milk infant formula unspiked and spiked at the 1 µg/kg (IS 10 µg/kg) level