AOAC 2018 Methods

Figure 201803A: GC-MS/MS chromatograms of sample Adult Nut 4 (unspiked). Quantification transitions for 3-MCPD, 2-MCPD and glycidol analysed as 3-MBPD above, and corresponding internal standards below.

3-MBPD 240 → 147.1

3-MCPD 196 → 147.1

2-MCPD 196 → 104

3-MCPD-d5 150 → 93

3-MBPD-d5 150 → 93

2-MCPD-d5 201 → 104.1