AOAC CASP Meeting - MYM 2020

7 Reference Material(s) See Tables 1 and 2 for sources of reference materials. Refer to Annex F: ' e Y e O o S ment and 8 se of , n + o X se 5 eference Mater L a O s in Appendix F: *XL de OL nes for Standard Method Performance 5 e TXL rements 2 f ¿ c L a O Methods of $ na O\ s L s of $2$& ,1 T (51$ T ,21$/ WK (G $2$& ,17(51$7,21$/ 5RFNYLOOH 0' 86$ KWWS ZZZ HRPD DRDF RUJ DSSBI SGI 8 Validation Guidance Appendix D: *XL de OL nes for & o OO a E orat LY e St X d \ Proced X res to 9 a OL date & haracter L st L cs of a Method of $ na O\ s L s 2 f ¿ c L a O Methods of $ na O\ s L s of $2$& ,1 T (51$ T ,21$/ WK (G $2$& ,17(51$7,21$/ 5RFNYLOOH 0' 86$ KWWS ZZZ HRPD DRDF RUJ DSSBG SGI Appendix F: *XL de OL nes for Standard Method Performance 5 e TXL rements 2 f ¿ c L a O Methods of $ na O\ s L s of $2$& ,1 T (51$ T ,21$/ WK (G $2$& ,17(51$7,21$/ 5RFNYLOOH 0' 86$ KWWS ZZZ HRPD DRDF RUJ DSSBI SGI AppendixK: *XL de OL nes for 'L etar \ S XSSO ements and % otan L ca O s 2 f ¿ c L a O Methods of $ na O\ s L s of $2$& ,1 T (51$ T ,21$/ WK (G $2$& ,17(51$7,21$/ 5RFNYLOOH 0' 86$ KWWS ZZZ HRPD DRDF RUJ DSSBN SGI 9 Maximum Time-to-Result 1RQH Approved by the AOAC Stakeholder Panel on Strategic Food Analytical Methods (SPSFAM) on March 13, 2017. Final Version Date: March 13, 2017.

Table 3. Method performance requirements (part 1) a

Required: THC, THCA, CBDA, CBD

Additional, desirable: Table 2, including CBN

Parameter

Limit of quantitation (LOQ; %, w/w)

”

”

Analytical range (%, w/w)

” ±FD

” ±FD

a Reported as individual cannabinoids.

Table 4. Method performance requirements (part 2)

Range (%, w/w)

” ±

! ±

! ±FD

Parameter

Recovery (%, w/w)

± ” ”

± ” ”

± ” ”

RSD r , % RSD R , %

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