AOAC CASP Meeting

7 Reference Material(s) See Tables 1 and 2 for sources of reference materials. Refer to Annex F: 'eYeOoSment and 8se of ,n +oXse 5eference MaterLaOs in Appendix F: *XLdeOLnes for Standard Method Performance 5eTXLrements 2f¿cLaO Methods of $naO\sLs of $2$& ,1T(51$T,21$/ WK (G $2$& ,17(51$7,21$/ 5RFNYLOOH 0' 86$ KWWS ZZZ HRPD DRDF RUJ DSSBI SGI 8 Validation Guidance Appendix D: *XLdeOLnes for &oOOaEoratLYe StXd\ ProcedXres to 9aOLdate &haracterLstLcs of a Method of $naO\sLs 2f¿cLaO Methods of $naO\sLs of $2$& ,1T(51$T,21$/ WK (G $2$& ,17(51$7,21$/ 5RFNYLOOH 0' 86$ KWWS ZZZ HRPD DRDF RUJ DSSBG SGI Appendix F: *XLdeOLnes for Standard Method Performance 5eTXLrements 2f¿cLaO Methods of $naO\sLs of $2$& ,1T(51$T,21$/ WK (G $2$& ,17(51$7,21$/ 5RFNYLOOH 0' 86$ KWWS ZZZ HRPD DRDF RUJ DSSBI SGI AppendixK: *XLdeOLnes for 'Letar\ SXSSOements and %otanLcaOs 2f¿cLaO Methods of $naO\sLs of $2$& ,1T(51$T,21$/ WK (G $2$& ,17(51$7,21$/ 5RFNYLOOH 0' 86$ KWWS ZZZ HRPD DRDF RUJ DSSBN SGI 9 Maximum Time-to-Result 1RQH Approved by the AOAC Stakeholder Panel on Strategic Food Analytical Methods (SPSFAM) on March 13, 2017. Final Version Date: March 13, 2017.

Table 3. Method performance requirements (part 1) a

Required: THC, THCA, CBDA, CBD

Additional, desirable: Table 2, including CBN

Parameter

Limit of quantitation (LOQ; %, w/w)

”

”

Analytical range (%, w/w)

” ±FD

” ±FD

a Reported as individual cannabinoids.

Table 4. Method performance requirements (part 2)

Range (%, w/w)

” ±

! ±

! ±FD

Parameter

Recovery (%, w/w)

± ” ”

± ” ”

± ” ”

RSD r RSD

, %

, %

R

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