AOAC CASP Meeting

5000

5000

150000

Propyl acetate

2500

Additional butane(sum of n- and iso-)

5000

5000

150000

2500

12

12

360

propane

6

2,2-dimethylbutane 2,3-dimethylbutane

290 290

290 290

145 145

8700 8700

2-butanone

5000 5000

5000 5000

2500 2500

150000 150000

2-methylbutane 2-methylpentane 3-methylpentane ethylbenzene ethylene oxide isobutane (methyl propane)

290 290

290 290

145 145

8700

8700

2170

2170

1085

65100

50

50

25

1500

12 12

12 12

6 6

360 360

n-butane n-heptane n-pentane

1000 1000

1000 1000

500 500

30000 30000

nitrogen o-xylene

0

0

0 5

10

10

300

triethylamine

5000

5000

2500

150000

50%

* USP Guidance (467) Residual Solvents

111 112 113

Table 2: Method performance requirements

Parameter

Requirement

LOQ* (ppm)

Specified in Table 1

Analytical Range (ppm)

LOQ to 100*LOQ specified in Table 1

114 115

Table 3: Method performance requirements for pesticides Residual Solvents in Table 1. Table 2:

Analytical Range

Parameters

100 to 500 ppm

1 to 100 ppm

500 to 1000 ppm