AOAC Final Action Methods in 2017

C ampos G iménez & M artin : J ournal of AOAC I nternational V ol . 101, N o . 4, 2018  1117

Table 3. Full set of raw data per sample and laboratory (samples 1 to 10) a Adult nutritional RTF b , high-fat SRM 1849a

Infant formula powder (FOS c /GOS d )

Soy-based infant formula Low-fat adult nutritional powder

Lab code

Sample 1 Sample 10 Sample 2 Sample 6 Sample 3 Sample 8 Sample 4 Sample 9 Sample 5 Sample 7

1 2 3 4 5 6 7 8 9

1.85 1.54 1.55 1.64 1.28 1.12 1.70 1.63 2.06 1.70 1.66 1.14 1.09 1.12 1.75 2.50 1.17

1.83 1.65 1.60 1.61 1.23 1.18 1.94 1.53 1.76 1.58 1.59 1.14 1.13 1.03 1.65 2.19 1.05

0.46 0.46 0.47 0.48 0.42 0.42 0.48 0.47 0.54 0.43 0.48 0.41 0.37 0.50 0.60 0.44

0.44 0.47 0.48 0.49 0.32 0.39 0.50 0.48 0.54 0.42 0.46 0.42 0.37 0.48 0.85 0.41

0.42 0.41 0.43 0.43 0.40 0.38 0.42 0.42 0.54 0.38 0.39 0.42 0.41 0.38 0.33 0.43 0.47 0.40

0.41 0.41 0.43 0.42 0.37 0.33 0.45 0.43 0.51 0.41 0.40 0.44 0.40 0.36 0.35 0.43 0.55 0.38

0.69 0.71 0.72 0.72 0.63 0.61 0.72 0.70 0.82 0.63 0.67 0.65 0.67 0.62 0.56 0.71 0.75 0.66

0.69 0.69 0.71 0.72 0.62 0.61 0.74 0.70 0.82 0.60 0.67 0.66 0.68 0.63 0.58 0.73 0.95 0.67

0.14 0.13 0.14 0.14 0.14 0.12 0.14 0.12 0.15 0.13 0.12 0.13 0.12 0.14 0.11 0.17 0.26 0.13

0.13 0.14 0.14 0.13 0.13 0.11 0.13 0.12 0.14 0.13 0.12 0.13 0.11 0.13 0.11 0.17 0.29 0.14

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10 11 12 13 14 15 16 17 18

Samples not received Samples not received

Samples not received

a Vitamin B

12 (cyanocobalamin) results in μg/100 g product as reconstituted or RTF.

b RTF = Ready-to-feed. c FOS = Fructooligosacchardides. d GOS = Galactooligosaccharides.

Table 4. Full set of raw data per sample and laboratory (samples 11 to 20) a Infant formula RTF b , milk-based Infant formula powder, part hydrolyzed milk-based Infant elemental powder

Infant formula powder, part hydrolyzed soy-based

Adult nutritional RTF, high-protein

Lab code Sample 11 Sample 13 Sample 12 Sample 16 Sample 14 Sample 20 Sample 15 Sample 18 Sample 17 Sample 19 1 0.22 0.23 0.37 0.35 0.70 0.71 0.28 0.29 1.31 1.32 2 0.23 0.23 0.35 0.35 0.71 0.69 0.27 0.26 1.14 1.20 3 0.22 0.23 0.35 0.34 0.76 0.77 0.27 0.26 1.18 1.22 4 0.22 0.23 0.36 0.37 0.72 0.72 0.28 0.27 1.25 1.23 5 0.20 0.21 0.34 0.32 0.60 0.61 0.25 0.24 1.09 1.01 6 0.19 0.19 0.32 0.29 0.64 0.65 0.25 0.25 1.08 1.11

Blank not subtracted nor reported

7 8 9

0.22 0.22 0.21

0.21 0.21 0.24

0.35 0.40 0.32 0.32 0.33 0.34 0.42 0.33 0.32 0.34 0.35 0.34

0.34 0.37 0.36 0.31 0.33 0.35 0.43 0.33 0.32 0.35 0.35 0.34

0.26 0.27 0.28

0.26 0.26 0.27

1.21 1.17 1.15 0.28 1.20 0.27 0.40 1.12 1.04 1.20 1.19 1.09

1.20 1.25 1.68 0.26 1.20 1.27 0.11 1.10 1.26 1.20 1.16 1.19

0.69 0.24

0.70 0.21

10 11 12 13 14 15 16 17 18

Samples not received

Samples not received

0.19 0.21

0.19 0.21

0.66

0.64

0.25

0.23 0.27

Sample not received Blank not subtracted nor reported

1.15 0.20 0.17 0.21 0.19 0.20

0.42 0.20 0.17 0.23 0.21 0.20

0.12 0.24 0.22 0.28 0.26 0.26

0.68 0.71 0.68 0.73 0.73

0.68 0.51 0.67 0.73 0.72

0.26 0.21 0.28 0.27 0.26

a Vitamin B

12 (cyanocobalamin) results in μg/100 g product as reconstituted or RTF.

b RTF = Ready-to-feed