AOAC Final Action Methods in 2017

548 P ACQUETTE & T HOMPSON : J OURNAL OF AOAC I NTERNATIONAL V OL . 101, N O . 2, 2018

Parameter 1 a 2 b 3 c 4 d 5 e 6 f 7 g 8 h 9 i 10 j 11 k 12 l 13 m 14 n 15 o 16 p 17 q 18 r Repeatability limit r (r = 2.8 × s r ) 0.00018 0.00140 0.00022 0.00077 0.00029 0.00011 0.00033 0.00015 0.00019 0.00013 0.00026 0.00021 0.00014 0.00028 0.00013 0.00033 0.00021 0.00021 Reproducibility limit R (R = 2.8 × s R ) 0.00051 0.00147 0.00048 0.00129 0.00029 0.00011 0.00073 0.00035 0.00041 0.00013 0.00030 0.00030 0.00023 0.00038 0.00023 0.00034 0.00026 0.00025 HorRat value 0.24 0.20 0.20 0.24 0.17 0.14 0.23 0.20 0.21 2.79 0.14 0.14 0.17 0.16 0.13 0.16 0.19 0.18 Repeatability limit SMPR 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 Reproducibility limit SMPR 15 15 15 15 15 15 15 15 15 15 15 15 15 15 15 15 15 15 a Adult Powder, Low-Fat. b Adult RTF, High-Fat. c Adult RTF, High-Fat Placebo. d Adult RTF, High-Protein. e Adult RTF, High-Protein Placebo. f Child Milk Powder Placebo. g Child Milk Powder. h Elemental Child Powder. i Infant Elemental Powder. j Infant Elemental Powder Placebo. k Infant Partly Hydrolyzed Powder Milk. l Infant Partly Hydrolyzed Powder Soy. m Infant Powder with fructo-oligosaccharides/galacto-oligosaccharides (FOS/GOS). n Infant Powder Milk. o Infant Powder Soy. p Infant RTF Milk. q Infant RTF Placebo. r Toddler Powder. s Parameters that failed SPIFAN SMPR criteria.

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Sample

Table 3. ( continued )

t The results are expressed in milligrams per 100 grams reconstituted final product (RTF liquids as-is; 25 g reconstituted powders in 200 g water). u No parameters failed SPIFAN SMPR criteria.