AOAC Final Action Methods in 2018
Table 2014.08D. Statistical results for the studied PAHs at three different concentration levels in oyster after elimination of statistical outliers
No. of laboratories
No. of replicates
Mean concn, µg/kg
Mean recovery, %
PAH
s r , µg/kg s R , µg/kg RSD r , % RSD R , % HorRat
1,7-DMP
8 8 8 8 9 9 7 8 8 7 7 7 9 9 9 7 7 6 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 8 9 9 9 9 9 9 9 9 9
16 16 16 16 18 18 14 16 16 14 14 14 18 18 18 14 14 12 18 18 18 18 18 18 18 18 18 18 18 18 18 18 18 18 18 18 18 16 18 18 18 18 18 18 18 18 18
72.3 69.0 65.6 67.9 90.8
90.4 86.2 82.0 90.5 90.8 94.6 80.8 79.8 77.3 76.2 77.2 71.7 92.5 88.6 87.5 53.2 50.3 56.6 72.6 68.6 71.6 49.7 48.2 49.3 85.9 81.8 82.8 82.4 81.9 78.4 85.9 84.3 83.8 85.9 81.6 81.6 82.7 82.2 80.0 83.3 81.2 76.0 88.2 83.9 80.5 86.8 83.3
4.1 4.9 5.5 4.3
11.7 12.6 13.2 14.8 28.9 55.3
5.7 7.1 8.4 6.4
16.2 18.3 20.1 21.8 31.9 23.4 23.9 19.3 22.4 17.5 18.6 13.0 13.0 13.0 12.0 55.0 64.7 44.5 19.7 21.1 17.5 43.5 42.2 40.5 11.6 11.2 11.9 12.3 13.6 11.7 16.3 15.4 13.1 13.0 13.4 12.7 15.4 14.6 19.9 16.2 17.9 14.2 13.1 13.7 9.9 10.6 9.3
0.68 0.76 0.83 0.91 1.39 1.18 0.83 0.74 1.06 0.65 0.76 0.62 0.47 0.55 0.59 1.56 1.94 1.67 0.62 0.71 0.73 1.10 1.18 1.45 0.35 0.40 0.51 0.34 0.41 0.41 0.48 0.52 0.54 0.39 0.45 0.46 0.35 0.41 0.43 0.50 0.51 0.81 0.57 0.69 0.65 0.36 0.42
1-MN
20.6 26.4
22.7 11.2
236.6
1-MP
20.2 39.9
1.8 2.6
4.8 7.7
8.8 6.4
154.7
16.9
34.7
10.9
2,6-DMN
30.5 57.9
3.0 4.9
5.3
9.8 8.5 7.9 6.0 6.4 5.1 8.8 8.8 7.7 5.8 5.4 9.0 6.4 6.6 7.1 4.1 5.9 8.6 4.9 7.7 6.5 6.1 6.5 6.2 4.3 9.0 7.5 4.4 8.2 6.8 4.0 9.5
10.8 20.9
161.3
12.7
3-MC
27.8 79.8
1.7 5.1
3.6
10.3 23.5
196.8
10.1
Ant
5.3 7.5
0.5 0.8 3.0 0.8 1.0 3.9 0.3 0.4 1.6 0.6 1.7 3.4 0.2 0.7 1.0 0.5 1.1 3.8 2.8 5.0 8.7 0.4 0.6 0.7 1.0 1.4 2.3 2.1 5.1 7.0 0.4 0.8
2.9 4.9
10.0
34.0 10.9 17.2 71.6
15.1
BaA
2.2 3.6
12.5
BaP
2.5 4.8
1.1 2.0
11.9
24.6
10.0
BbF
8.6
1.0 2.7 9.8 0.5 1.1 2.3 1.1 2.6 8.2 4.3 8.6 0.5 1.1 2.0 1.9 3.0
24.6 82.8
BghiP
4.1 8.2
19.6
BkF
6.9
16.9 62.9 43.0 81.6
Chr
204.1
19.0
DBahA
4.1 8.2
16.0 12.5 20.3 57.0 22.0 42.0
Fln
11.3
Flt
3.6 7.5
12.2
120.7
17.1
5.8 9.6 9.0
IcdP
4.3 8.3
0.6 1.1
© 2015 AOAC INTERNATIONAL
Made with FlippingBook HTML5