AOAC ISPAM Food Allergens Egg/Milk SMPR Info to WG

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Table 1: Method performance requirements

Parameter

Minimum Acceptance Criteria for target matrix

Analytical Range (ppm) 1

≤10 - ≥ 20 2

LOQ (ppm) 1

≤10

LOD (ppm) 1

≤10

50-150%

Recovery (%) 3

% RSD r

≤20 %

% RSD

≤30%

R

Notes: 1 ppm in non-fat dried milk. 2 See Annex 1 for rationale for setting lower limit of range. 3 Use incurred samples as per Appendix M. Incurred materials can be obtained from MoniQA Association.

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1. Appendix M: 20th Edition of the Official Methods of Analysis of AOAC INTERNATIONAL (2016); and Validation procedures for quantitative food allergen ELISA methods: Community guidance and best practices . Journal of AOAC INTERNATIONAL [93(2) 442-450] (2010)

2. Ibid. 3. Ibid. 4. ISO 5725-1:1994 5 I bid.