AOAC ISPAM Meeting eBook, March 17 2015

DuPont/Campden Data

Concentrati on

FDA-BAM Reference

ISO Reference

Matrix

N

dPOD C

95% CI

MPN/25g

X

POD C

95% CI 0.00,0.46

x

POD R

95% CI 0.00,0.46

0.00

5

0

0.00

0

0.00

0.00

-0.43,0.43

Seafood (prawns)

0.375

20

5

0.25

0.11,0.47

2

0.10

0.028,0.30

0.15

-0.09,0.38

1.075

20

15

0.75

0.53,0.89

15

0.75

0.53,0.89

0.00

-0.26,0.26

0.00

5

0

0.00

0.00,0.46

0

0.00

0.00,0.46

0.00

-0.43,0.43

Spice (black pepper)

6

20

19

0.95

0.76,0.99

20

1.00

0.84,1.00

-0.05

-0.24,0.12

10.75

20

20

1.00

0.84,1.00

20

1.00

0.84,1.00

0.00

-0.16,0.16

0.00

5

0

0.00

0.00,0.46

0

0.00

0.00,0.46

0.00

-0.43,0.43

Dry Pet Food

0.575

20

13

0.65

0.43,0.82

19

0.95

0.76,0.99

-0.30

-0.52, -0.049

2.325

20

20

1.00

0.84,1.00

19

0.95

0.76,0.99

0.05

-0.12,0.24

0.00

5

0

0.00

0.00,0.46

0

0.00

0.00,0.46

0.00

-0.43,0.43

Raw Pizza Dough

0.95

20

11

0.55

0.34,0.74

18

0.90

0.70,0.97

-0.35

-0.57, -0.072

23.25

20

18

0.90

0.70,0.97

20

1.00

0.84,1.00

-0.10

-0.30,0.077

Egg and Cress Sandwiche s

0.00

5

0

0.00

0.00,0.46

0

0.00

0.00,0.46

0.00

-0.43,0.43

<0.075

20

20

1.00

0.84,1.00

13

0.65

0.43,0.82

0.35

0.11,0.57

9.5

20

16

0.80

0.58,0.92

20

1.00

0.84,1.00

-0.20

-0.42,0.0005

Chilled Dairy Desert (custard ) Chilled Dairy Desert (custard)

0.00

5

0

0.00

0.00,0.46

0

0.00

0.00,0.46

0.00

-0.43,0.43

18.75

20

20

1.00

0.84,1.00

20

1.00

0.84,1.00

0.00

-0.16,0.16

60.0

20

20

1.00

0.84,1.00

20

1.00

0.84,1.00

0.00

-0.16,0.16

0.00

5

0

0.00

0.00,0.46

0

0.00

0.00,0.46

0.00

-0.43,0.43

6.0

20

15

0.75

0.53,0.89

15

0.75

0.53,0.89

0.00

-0.26,0.26

Annex A “Classification of sample types and suggested target combinations for validation studies”

• 18 categories

– Raw milk and dairy products (4) – Heat processed milk and dairy products – Raw meat and ready-to-cook meat products (except poultry) – Ready-to-eat, ready-to-reheat meat products – Raw poultry and ready-to-cook poultry products (1) – Ready-to-eat, ready-to-reheat meat poultry products – Eggs and derivatives (1) – Raw and ready-to-cook fish and seafood (unprocessed) (1) – Ready-to-eat, ready-to-reheat fishery products

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