AOAC RI Chemical Cont. Methods-2018 Awards
666 S chneider & A ndersen : J ournal of AOAC I nternational V ol . 98, N o . 3, 2015
Table 6. Residue identification summary Analytes identified, %, n = 28
Table 6. ( continued )
Analytes identified, %, n = 28
Concn of analytes, µg/kg
Concn (>0.05 μg/kg) of analytes in individual blank samples c , μg/kg
Concn of analytes, µg/kg Incurred
Concn (>0.05 μg/kg) of analytes in individual blank samples c , μg/kg
EU a
FDA b
EU a
FDA b
Analyte Matrix
Analyte Matrix
MG Salmon Blank
7
7
0.10, 0.11
89
93
0.42
93
93
Shrimp Blank
46
46
0.30
0.90
100 100
0.42
100 100
1.75 100 100 Incurred 100 100
0.90
100
96
1.75 100 100 Incurred 100 100
Catfish Blank
0
0
0.42
96
100
LCV Salmon Blank
50
43
0.06, 0.08
0.90
93
93
0.42
100
86
1.75
100 100
0.90
100 100
Incurred
93
100
1.75
100 100
Shrimp Blank
4
4
Incurred 100
96
0.42
100 100
Catfish Blank
33
22
0.08, 0.12, 0.13
0.90
100 100
0.42
100 100
1.75
93
93
0.90
96
96
Incurred
82
89
1.75
100 100
LMG Salmon Blank
4
4
0.08
Incurred
93
93
0.42
100 100
Shrimp Blank
0
0
0.90
100 100
0.42
93
93
1.75 100 100 Incurred 100 100
0.90
93
86
1.75
93
89
Catfish Blank
11
11
Incurred
96
89
0.42
100 100
BG Salmon Blank
18
18
0.13
0.90
100 100
0.42
93
89
1.75 100 100 Incurred 100 100
0.90
96
96
1.75 100 100 Incurred 100 100
Shrimp Blank
0
0
0.42
100 100
Catfish Blank
15
15
0.08, 0.08
0.90
100 100
0.42
100 100
1.75 100 100 Incurred 100 100
0.90
100 100
1.75 100 100 Incurred 100 100
CV Salmon Blank
57
57
0.14
0.42
100 100
Shrimp Blank
14
14
0.90
100 100
0.42
96
96
1.75
100 100
0.90
100 100
Incurred
79
79
1.75 96 Incurred 100 100 96
Catfish Blank
76
76
a ±20–50% relative, based on value. b ±10% absolute. c Only blank samples that meet confirmation criteria for the analyte/matrix pair and have a calculated concentration >0.05 μg/kg are reported.
0.42
100 100
0.90
100 100
1.75
100 100
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