AOAC-RI ERP Book - FAOM METHOD.pdf
502 M ASTOVSKA ET AL . J OURNAL OF AOAC I NTERNATIONAL V OL . 98, N O . 2, 2015
7DEOH –20°C PAH
5HFRYHULHV RI WKH VWXGLHG 3$+V LQ R\VWHU REWDLQHG E\ D FROODERUDWRU VWRULQJ WKH WHVW VDPSOHV 6)& 2 ±2 DW
SFC O1
SFC O2
SFC O3
SFC O4
SFC O5
SFC O6
SFC O7
Mean
RSD, %
1,7-DMP
93
95
93
102
90
107
92
96
1-MN 1-MP
102
102
98
124
98
111
106
97 85 92 41 74 47 82 87 86 86 87 86 85 88 93 89 86
99 77 94 47 75 51 88 83 85 85 84 86 84 85 93 87 85
100
93 65 96 50 78 52 87 82 89 87 82 83 87 86 95 90 88
109
94 73 96 44 76 50 86 90 88 87 86 86 91 89 94 88 85
99 77 95 48 77 52 87 86 88 87 85 85 87 87 95 89 87
2,6-DMN
91 98 51 80 56 92 87 92 91 89 93 90 88
71 97 53 81 54 89 84 89 88 84 77 88 86 92 89 88
13
3-MC
9.6
Ant
BaA BaP BbF
6.3
BghiP
BkF Chr
DBahA
Fln
Flt
IcdP Naph
101
Phe Pyr
93 89
7DEOH –70°C PAH
5HFRYHULHV RI WKH VWXGLHG 3$+V LQ R\VWHU REWDLQHG E\D FROODERUDWRU VWRULQJ WKH WHVW VDPSOHV 6)& 2 ±2 DW
SFC O1 SFC O2 SFC O3 SFC O4 SFC O5 SFC O6 SFC O7 Mean RSD, %
1,7-DMP
94
99
108
95
98
106 101 102
96
100 106
1-MN 1-MP
107
109 100
109 100
110
101
94 85 99 92 88 90 90 94 91 90 95 93 95 94 94 90 92
92 80 96 87 87 85 87 89 90 88 92 88 88 87 93 89 90
88 78 93 84 81 82 83 90 85 84 89 87 86 87 88 84 86
96 83 99 89 88 86 90 93 90 90 94 91 91 91 94 90 91
2,6-DMN
90
89
77
3-MC
101
102
100
91 90 87 93 95 92 92 96 94 92 93 99 92 94
89 90 86 93 94 91 92 95 93 94 93 96 91 93
Ant
91 91 88 92 94 94 93 96 92 92 92 96 93 94
BaA BaP BbF
BghiP
BkF Chr
DBahA
Fln
Flt
IcdP Naph
Phe
Pyr
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