AOAC-RI ERP Book - FAOM METHOD.pdf
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No. of laboratories
No. of replicates
Mean concn, μg/kg
Mean recovery, % s r
PAH
, μg/kg s R
, μg/kg RSD r
, % RSD R
, % HorRat
1,7-DMP
9 9 9 9 9 9 9 9 9 8 8 7 9 9 9 9 9 9 9 9 9 9 9 8 9 9 9 8 8 8 9 9 9 8 9 9 9 9 9 8 9 9 9 9 9 9 9
18 18 18 18 18 18 18 18 18 16 16 14 18 18 18 18 18 18 18 18 18 18 18 16 18 18 18 16 16 16 18 18 18 16 18 18 18 18 18 16 18 18 18 18 18 18 18
21.7 22.7 21.7 23.1 81.5
108.6 113.7 108.3 115.4 108.6 101.6
2.6 1.8 1.9 6.2 6.7 1.0 1.9 6.7 1.1 4.8 0.6 1.6 8.7 0.3 0.8 2.4 0.3 0.6 2.5 0.1 0.4 1.1 0.3 0.3 3.9 0.1 0.2 1.0 0.1 0.4 1.8 0.5 2.2 9.0 0.2 0.3 0.9 0.1 0.6 2.1 0.6 1.4 4.9 0.1 0.5
4.1 4.2 4.4 6.8
11.8
18.9 18.7 20.4 29.4 19.1 27.3 14.0 14.9 13.1 16.4 19.5 13.9 13.1 11.1 10.3 16.2 11.7 9.4
0.66 0.66 0.72 1.04 0.82 1.34 0.44 0.53 0.60 0.55 0.74 0.65 0.42 0.42 0.44 0.29 0.51 0.45 0.27 0.28 0.37 0.29 0.27 0.25 0.28 0.22 0.37 0.28 0.28 0.27 0.34 0.26 0.28 0.31 0.32 0.41 0.33 0.32 0.28 0.28 0.25 0.34 0.32 0.35 0.41 0.32 0.31
8.0 8.8
1-MN
26.9
15.6 55.4
8.3 8.8 9.8 7.6 5.6 6.9 5.8 5.1 6.0 6.7 7.3 6.2 7.0 4.3 4.5 6.5 7.3 4.6 6.6 2.6 5.5 7.0 4.3 5.7 6.2 4.9 4.7 3.1 4.4 5.3 6.6 6.4 1.4 4.2 4.5 6.0 5.5 5.2 5.3 9.1
203.2
17.8
1-MP
10.0 25.0
99.9 99.9 95.5
1.4 3.7
119.4
15.7
2,6-DMN
15.6 37.8
103.9
2.6 7.4
94.6 83.8
12.6 11.3
146.7
16.6
20.3
6-MC
11.1 32.2
110.5 107.2 100.1
1.5 3.6
145.2
13.7
Ant
4.9
98.5
0.5 1.7 4.6 0.5 1.3 5.2 0.2 0.5 1.6 0.5 0.7 6.3 0.2 0.5 1.4 0.3 0.7 2.8 1.4 4.1 0.3 0.6 1.2 0.5 1.1 4.1 1.0 2.4 8.7 0.3 0.6
10.6 38.9
105.7
97.4 95.9 99.9 94.4 96.2 98.7 92.3 96.7 98.2 95.5 94.7 98.5 90.1 99.5
BaA
4.8
9.7 8.4 9.2
15.0 56.6
BaP
1.9 4.9
12.1
9.6 7.0
23.1
BbF
4.8 9.8
10.1
7.0 8.8
71.6
BghiP
1.9 4.9
11.7
9.9 7.9
18.0
BkF
2.0 8.1
13.7
101.7
8.7 7.2 9.4 8.1 8.7
38.3 15.2 50.7
95.8
Chr
101.5 101.4
167.4
95.6 95.9
14.5
DBahA
1.9 5.0
10.9
13.5 11.2
100.4
13.8
91.8
8.4
Fln
5.2
103.0 102.3
10.0
15.4 47.3
7.5 8.7
94.7 97.2
Flt
9.7
10.4
25.1 93.9
100.3
9.7 9.3
93.9 98.2
IcdP
2.0 5.1
13.3 11.0
102.2
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