AOAC-RI ERP Book - FAOM METHOD.pdf

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N o . of laboratories

No. of replicates

Mean concn, μg/kg

Mean recovery, %

PAH

s r , μg/kg s R

, μg/kg RSD r

, % RSD R

, % HorRat

1,7-DMP

8 8 8 8 9 9 7 8 8 7 7 7 9 9 9 7 7 6 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 8 9 9 9 9 9 9 9 9 9

16 16 16 16 18 18 14 16 16 14 14 14 18 18 18 14 14 12 18 18 18 18 18 18 18 18 18 18 18 18 18 18 18 18 18 18 18 16 18 18 18 18 18 18 18 18 18

72.3 69.0 65.6 67.9 90.8

90.4 86.2 82.0 90.5 90.8 94.6 80.8 79.8 77.3 76.2 77.2 71.7 92.5 88.6 87.5 53.2 50.3 56.6 72.6 68.6 71.6 49.7 48.2 49.3 85.9 81.8 82.8 82.4 81.9 78.4 85.9 84.3 83.8 85.9 81.6 81.6 82.7 82.2 80.0 83.3 81.2 76.0 88.2 83.9 80.5 86.8 83.3

4.1 4.9 5.5 4.3

11.7 12.6 13.2 14.8 28.9 55.3

5.7 7.1 8.4 6.4

16.2 18.3 20.1 21.8 31.9 23.4 23.9 19.3 22.4 17.5 18.6 13.0 13.0 13.0 12.0 55.0 64.7 44.5 19.7 21.1 17.5 43.5 42.2 40.5 11.6 11.2 11.9 12.3 13.6 11.7 16.3 15.4 13.1 13.0 13.4 12.7 15.4 14.6 19.9 16.2 17.9 14.2 13.1 13.7 9.9 10.6 9.3

0.68 0.76 0.83 0.91 1.39 1.18 0.83 0.74 1.06 0.65 0.76 0.62 0.47 0.55 0.59 1.56 1.94 1.67 0.62 0.71 0.73 1.10 1.18 1.45 0.35 0.40 0.51 0.34 0.41 0.41 0.48 0.52 0.54 0.39 0.45 0.46 0.35 0.41 0.43 0.50 0.51 0.81 0.57 0.69 0.65 0.36 0.42

1-MN

20.6 26.4

22.7 11.2

236.6

1-MP

20.2 39.9

1.8 2.6

4.8 7.7

8.8 6.4

154.7

16.9

34.7

10.9

2,6-DMN

30.5 57.9

3.0 4.9

5.3

9.8 8.5 7.9 6.0 6.4 5.1 8.8 8.8 7.7 5.8 5.4 9.0 6.4 6.6 7.1 4.1 5.9 8.6 4.9 7.7 6.5 6.1 6.5 6.2 4.3 9.0 7.5 4.4 8.2 6.8 4.0 9.5

10.8 20.9

161.3

12.7

3-MC

27.8 79.8

1.7 5.1

3.6

10.3 23.5

196.8

10.1

Ant

5.3 7.5

0.5 0.8 3.0 0.8 1.0 3.9 0.3 0.4 1.6 0.6 1.7 3.4 0.2 0.7 1.0 0.5 1.1 3.8 2.8 5.0 8.7 0.4 0.6 0.7 1.0 1.4 2.3 2.1 5.1 7.0 0.4 0.8

2.9 4.9

10.0

34.0 10.9 17.2 71.6

15.1

BaA

2.2 3.6

12.5

BaP

2.5 4.8

1.1 2.0

11.9

24.6

10.0

BbF

8.6

1.0 2.7 9.8 0.5 1.1 2.3 1.1 2.6 8.2 4.3 8.6 0.5 1.1 2.0 1.9 3.0

24.6 82.8

BghiP

4.1 8.2

19.6

BkF

6.9

16.9 62.9 43.0 81.6

Chr

204.1

19.0

DBahA

4.1 8.2

16.0 12.5 20.3 57.0 22.0 42.0

Fln

11.3

Flt

3.6 7.5

12.2

120.7

17.1

5.8 9.6 9.0

IcdP

4.3 8.3

0.6 1.1

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