AOAC-RI ERP Book - FAOM METHOD.pdf

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Repeatabili LOQ (μg/kg) Linearity range (μg/kg) Naph 77 80 81 77 86 67 78 9 0.1 0.10 - 100 ty, RSD (%)

Ace 72 79 82 84 75 84 79 6 0.1 0.10 - 100

Fln 80 79 80 93 79 87 83 7 0.05 0.05 - 100

Phe 80 72 87 86 68 80 79 9 0.05 0.05 - 100

Ant 75 73 76 85 74 85 78 7 0.05 0.05 - 100

Flt 100 87 101 97 96 103 97 6 0.05 0.05 - 100

Pyr 89 78 82 93 80 89 85 7 0.05 0.05 - 100

BaA 82 88 83 92 82 89 86 5 0.05 0.05 - 100

Chr 84 79 84 96 83 91 86 7 0.05 0.05 - 100

BbF 84 82 87 98 81 93 88 8 0.05 0.05 - 100

BkF 87 84 90 100 85 97 91 7 0.05 0.05 - 100

BaP 87 84 89 99 84 95 90 7 0.05 0.05 - 100

DBahA 89 85 91 100 87 97 91 6 0.05 0.05 - 100

BghiP 88 85 91 99 87 97 91 6 0.05 0.05 - 100

IcdP 89 86 92 100 86 100 92 7 0.05 0.05 - 100

Validation data – method performance characteristics Shrimps – spiked concentrations – 1 and 5 μg/kg Concentration level 1 μg/kg Analyte Spike 1 Spike 2 Spike 3 Spike 4 Spike 5 Spike 6 Recovery (%)