AOAC-RI ERP Book - FAOM METHOD.pdf

M ASTOVSKA ET AL .: J OURNAL OF AOAC I NTERNATIONAL V OL . 98, N O . 2, 2015 491

Table 2014.08H. MS ions ( m / z ) and MS/MS precursor to product ion transitions used by study participants for TXDQWL¿FDWLRQ TXDQW DQG LGHQWL¿FDWLRQ TXDO RI WDUJHW 3$+V DQG 13 C -PAHs using single-stage MS (single quadrupole and 72) DQG WDQGHP 06 06 WULSOH TXDGUXSROH LQVWUXPHQWV UHVSHFWLYHO\ 6LQJOH TXDG 72) 06 7ULSOH TXDG 06 06 &RPSRXQG 4XDQW 4XDO 4XDQW 4XDO 1,7-DMP 206 191 206>190 206>205, 206>165 1-MN 142 115 142>115 142>141, 142>116 1-MP 192 189 192>191 192>165 2,6-DMN 156 141, 144 156>115 156>141 3-MC 242 241 242>239 242>226 Ant 178 177 178>176 178>177, 178>151 BaA 228 226 228>226 228>224, 228>202 BaP 252 253 252>250 250>248, 252>224 BbF 252 253 252>250 250>248, 252>224 BghiP 276 277 276>274 274>272, 276>275 BkF 252 253 252>250 250>248, 252>224 Chr 228 226 228>226 228>224, 228>202 DBahA 278 276 278>276 276>274, 278>274 Fln 166 165 166>165 166>164, 166>163 Flt 202 200 202>200 202>201 IcdP 276 277 276>274 274>272, 276>248 Naph 128 127 128>102 128>127 Phe 178 177 178>176 178>177, 178>151 Pyr 202 200 202>200 202>201 13C-Ant 184 183 184>183 184>182, 184>156 13C-BaA 234 232 234>232 234>206 13C-BaP 256 257 256>254 256>228 13C-BbF 258 259 258>256 258>255 13C-BghiP 288 289 288>286 288>287 13C-BkF 258 259 258>256 258>255 13C-Chr 234 232 234>232 234>206 13C-DBahA 284 282 284>282 284>280 13C-Fln 172 171 172>171 172>170 13C-Flt 208 205 208>206 208>207 13C-IcdP 282 283 282>280 282>281 13C-Naph 134 133 134>133 134>105 13C-Phe 184 183 184>183 184>156 13C-Pyr 205 203, 206, 208 205>203 205>204

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