AOAC RI ERP EBOOK FOR FERTILIZERS
Author Response to Reviewers 071506_OMAMAN-28-AOAC 2006.03_rev 071816
Table 7. Method precision and comparability to 2006.03, revised. Proposed method (n=3) Collaborative study 2006.03 results Material Avg., mg/kg RSD, % Avg., mg/kg RSDr, %
Recovery, %
Horrat(r)
As
A B C D E
41.49
1.86 1.39 3.05 3.43 0.62 2.10 0.35 3.32 1.77 2.23 2.23 1.45 1.82 4.95 3.73 NA
22.15 263.2 4.87 4945 2432 9.75 22.43
42.93 47.96 63.12
187.32 181.95 141.42 119.67 121.45 106.26
0.58 0.62 0.72 2.24 0.36 0.54 0.10 0.70 0.46 0.86 0.86 0.36 0.50 1.08 1.22 0.80 1.78 0.50 1.28 1.90 0.30 0.48 0.30 NA
478.89
6.89
5917.76 2953.58
6.09
10.56 41.73
F
10.36 22.32
G H
9.36 17.6
99.49
2.92
2.36
123.63
I J
11.95
13.04
13.27
91.63
189.46 168.49
185.45 175.28
4.27 7.84
102.16
K L
96.13
bdl
NA
NA
NA
M
9.31
7.35
53.17 15.74 45.14
126.64 136.62
N O
17.41
12.74
3.77
4.16
90.66
P
60.72
47.83
2.22
126.94
Cd A
2.40 5.29
3.92 7.83 1.79 4.04 6.51 0.76 1.61
2.25 7.56
39.14 19.65
106.78
B C D E
69.97
22.07 44.91 27.86
21.28 36.64 22.58 214.6 26.69 55.29
0.61
103.72 122.56
3.2
4.25 3.06 5.79 1.25
123.4
F
235.39
109.69 107.65 115.00
G H
28.73 63.58
0.9 NA
I J
bdl
NA
NA
NA
NA
16.65 66.05
0.44 2.29
15.52 64.04
2.77 2.95
107.26 103.14
0.12 0.76
K L
bdl
NA
NA
NA
NA
NA
M
4.32
9.64
4.19
3.18
103.17
2.14
N O
bdl bdl
NA NA
NA NA
NA NA
NA NA
NA NA
P
0.52
20.46
0.57
66.74
92.02
1.88
Co
A
119.71
2.69
97.75
4.12
122.47
0.98
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