AOAC SPIFAN Nutrients ERP (December 7, 2022)

Fluor-06 (SLV) 10-2022 FOR ERP USE ONLY DO NOT DISTRIBUTE

Table of Contents

1

Summary ..........................................................................................................................3

2

Company and team members ...........................................................................................4 Company information .............................................................................................................. 4 Team members ........................................................................................................................ 4

2.1 2.2

3

Introduction .....................................................................................................................5

4

Method ............................................................................................................................6 Principle ................................................................................................................................... 6 Apparatus................................................................................................................................. 7 Reagents, materials and safety precautions............................................................................ 7 Preparation of standard and calibration solutions .................................................................. 7 Calculations .............................................................................................................................. 8 Preparation of test sample ...................................................................................................... 8 Samples .................................................................................................................................... 9 System suitability ..................................................................................................................... 9 Acceptance criteria .................................................................................................................. 9 Results............................................................................................................................11 Linearity ................................................................................................................................. 11 Limit of quantification (LOQ) ................................................................................................. 12 Specificity and selectivity ....................................................................................................... 12 Recovery ................................................................................................................................ 14 Accuracy................................................................................................................................. 15 Repeatability .......................................................................................................................... 15 Reproducibility ....................................................................................................................... 16 Robustness ............................................................................................................................. 17

4.1 4.2 4.3 4.4 4.5 4.6 4.7 4.8 4.9 5.1 5.2 5.3 5.4 5.5 5.6 5.7 5.8 5

6

References......................................................................................................................19

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