AOAC SPIFAN Nutrients ERP-Final Review (Oct. 2018) Pubs

2011.14 (Oct. 2018) – MTE-03 Manuscript Tables Final Action Review FOR ERP USE ONLY DO NOT DISTRIBUTE

2011.14 Manuscript Tables

Table 1. SMPR 2014.004 Requirements Parameter a Mn Lower analytical range, mg/100 g 0.001 0.001 Cu

Fe

Zn 0.1 18 0.1

Mg

P

Na 10 850

Ca 20

K

0.01

3

15

10

Upper analytical range, mg/100 g

1.0

1.2

20

110

800

1280

2000

LOQ, mg/100 g Recovery, %

0.001 0.001

0.01

3

15

10

20

10

90-110% of mean spiked recovery over the range of the assay

RSD r , % RSD R , %

5

”0.005 mg/100 g >0.005 mg/100 g

”

” a Concentrations apply to: (a) “ready to feed” liquids “as is”; (b) reconstituted powders (25 g into 200 g of water); and (c) liquid concentrates diluted 1:1 by weight.