AOAC SPIFAN Nutrients ERP Review (March 14, 2019)

Appendix C2. Sample Milumil

Column info

spike (mg) (spike stock solution 10 mg/kg)

Sample run no. refers to independent analyses on individual days

column #1 A Supp 16 S/N 022.3157, column #2 A Supp 16 S/N 0102.3039 column #1 column #1 column #1 column #1 column #1 column #1 column #1 column #1 column #1 column #2 column #2 column #2 column #2

Calibration Anions_low, quadratic through 0, unweighted

SD F- FIN (µg/100 g)

Spike concentration (μg/100 g)

F- (µg/100 g) (1)

F- (µg/100 g) (1)

F- FIN (µg/100 g) AVG

Analyst sample preparation

RSD (%)

Sample info

Milumil A3_#1 A3_#2 A3_#3 A3_#4 A3_#4 A3_#4 A3_#5 A3_#5 A3_#5 A3_#6 A3_#7 A3_#7 A3_#7

calibration 1, analyst 1 calibration 1, analyst 1 calibration 1, analyst 1 calibration 1, analyst 1 calibration 1, analyst 1 calibration 1, analyst 1 calibration 2, analyst 2 calibration 2, analyst 2 calibration 2, analyst 2 calibration 3, analyst 2 calibration 3, analyst 2 calibration 3, analyst 2 calibration 3, analyst 2

analyst 1 analyst 1 analyst 1 analyst 2 analyst 2 analyst 2 analyst 2 analyst 2 analyst 2 analyst 2 analyst 2 analyst 2 analyst 2

sample sample sample sample

60.4 60.9 57.4 59.1 73.8 91.3 50.8 61.5 82.5 75.5 67.4 84.4

61.1 62.4 57.9 58.3 75.9 93.5 52.6 64.0 83.7 74.3 69.8 86.5

60.8 61.6 57.6 58.7 74.8 92.4 51.7 62.8 83.1 74.9 68.6 85.4

0.5 1.1 0.3 0.6 1.5 1.6 1.3 1.7 0.9 0.9 1.7 1.5 0.6

0.8 1.7 0.5 1.0 2.0 1.7 2.5 2.7 1.1 1.2 2.5 1.8 0.6

sample + spike sample + spike

48 98

19.2 39.1

sample

sample + spike sample + spike

47 98

18.6 39.4

sample sample

sample + spike sample + spike

48 99

19.0 39.5

101.9

102.8

102.4

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