AOAC SPIFAN Nutrients ERP Review (March 14, 2019)

2016.13 (Jan. 2019) Carot-02 MLT Report FOR ERP USE ONLY DO NOT DISTRIBUTE

Table 7. Raw data for all- trans -β-carotene in fortified formulas, expressed as µg/100 g reconstituted basis

Milk-based toddler formula powder

Elemental infant formula powder d UOPM297/ ECHL425

Milk-based infant formula powder

Soy-based infant formula powder

Milk-based infant formula powder

NIST SRM 1869 GBAN911/ PTLO721

Infant formula ready-to-feed

EFXN778/ BFAO941

JSDT587/ NSRB999

TJHR217/ OACN211

CULF358/ GBZC169

CMJC380/ ETVZ191

Lab number

1 2 3 4 5 6 7 8 9

6.74 7.11

6.63 7.29

7.58

7.57 14.36 6.18

9.60

9.62

11.14 11.18 12.73 12.62 14.68 14.78

8.07 7.57 15.79 9.30 12.19 a 10.65 a 13.70 a 7.74 a 15.16 14.52 17.46 17.64

8.07 a 10.06 a 8.98

9.71

7.60 13.89 7.94

8.35

9.72 10.22 10.12 a 9.30 a 11.99 a 11.74 a

7.60 6.67 6.46 6.56 6.82 6.88

8.30 6.76 6.47 6.40 6.76 6.61

7.97 a 8.77 a 16.36 13.71 11.19 11.01 12.58 12.45 14.93 14.56 17.92 17.20

7.37 7.55 7.11

7.55 11.80 15.28 9.90

10.01 11.24 12.22 13.06 12.90 15.71 15.70 11.11 11.26 13.81 13.90 16.54 16.11 9.96 10.46 11.88 12.29 13.35 13.12 9.89 8.99

7.41 6.81

7.54 14.79 9.65 5.53 14.52 9.21

6.26 6.98 15.33 8.11 11.06 11.05 12.77 12.63 14.10 14.67 17.13 16.22

8.37

7.95 16.17 13.36 9.95

9.90

11.50 11.38 13.17 13.06 15.29 15.18

10 9.06 c 8.63 c 11.26 b 11.82 b 18.22 16.25 13.99 13.31 15.10 13.51 17.56 18.36 22.69 a 22.32 a a Cochran outlier

b Single Grubbs outlier c Double Grubbs outlier d Post hoc homogeneity testing showed the sample to be non-homogeneous. See Appendix B.

15