AOAC SPIFAN Stakeholder Panel (August 25, 2018)

SMPR: 2-MCPD

Parameter

2-MCPD * in dry infant formula samples (powder)

2-MCPD* in liquid infant formula samples

Analytical range (ʅŐ/kg)

25 – ш ϱϬϬ

3 – ш ϲϬ

LOQ (ʅg/kg)

ч Ϯϱ

ч ϯ

Accuracy (%)

70-125

70-125

ч ϮϮ

ч ϮϮ

% RSD r

25-100 ʅg/kg ч ϰϰ

% RSD R

ч ϰϰ

хϭϬϬ ʅg/kg

ч Ϯϱ

* Total analyte content expressed as free 2-MCPD resulting either from separate or from combined determination of free 2-MCPD and bound 2-MCPD.

SMPR: Glycidol

Parameter

Glycidol* in dry infant formula samples (powder)

Glycidol* in liquid infant formula samples

Analytical range (ʅŐ/kg)

15 – ш ϰϬϬ

2 – ш ϰϴ

LOQ (ʅg/kg)

ч ϭϱ

ч Ϯ

Accuracy (%)

70-125

70-125

ч ϮϮ

ч ϮϮ

% RSD r

15-ϰϴ ʅg/kg

ч ϰϰ

% RSD R

ч ϰϰ

>ϰϴ ʅg/kg

ч Ϯϱ

* Analyte content resulting from the determination of bound glycidol .