AOAC SPIFAN Stakeholder Panel Meeting Book (September 7, 2019)

Analytical Data LOD/LOQ Na Mg P K

Ca

Mn

Fe

Cu

Zn

Cr

Se

Mo

DAY 1 -0.002142 -0.000191 -0.001660 -0.000586 -0.001709 0.000008 0.000302 0.000008 0.004890 -0.000000691 -0.000009228 0.000003360 DAY 2 -0.000162 0.001556 -0.000133 0.006475 0.001214 -0.000027 -0.000012 0.000024 0.000369 -0.000017715 -0.000008157 0.000007865 DAY 3 -0.000661 0.000759 -0.001299 0.006220 0.012982 0.000031 0.000309 0.000052 -0.001187 0.000002580 0.000004832 0.000003079 DAY 4 -0.002044 0.000257 -0.000492 -0.002640 0.008721 0.000036 0.000621 0.000044 -0.000753 0.000003739 0.000016000 0.000001000 DAY 5 -0.000794 0.000690 0.001867 0.005627 0.008484 0.000030 0.000431 0.000059 0.000207 0.000015421 0.000011292 0.000010979 MEAN -0.00116060 0.00061420 -0.00034340 0.00301920 0.00593840 0.00001560 0.00033020 0.00003740 0.00070520 0.00000067 0.00000295 0.00000526 SD 0.0008838 0.0006499 0.0013783 0.0043015 0.0060133 0.0000261 0.0002308 0.0000210 0.0024280 0.0000119 0.0000113 0.0000041 LOQ μg/g 0.00768 0.00711 0.01344 0.04603 0.06607 0.00028 0.00264 0.00025 0.02499 0.00012 0.00012 0.00005 LOQ mg/100g 0.0383893 0.0355675 0.0671979 0.2301720 0.3303558 0.0013850 0.0131909 0.0012380 0.1249255 0.0006005 0.0005821 0.0002294 SMPR mg/100g 10 3.0 15 10 20 0.001 0.010 0.001 0.10 0.002 0.001 0.002

Analytical Data SRM 1849a Results (mg/kg) Na Mg P K Ca Mn

Fe

Cu

Zn

Cr

Se

Mo

DAY 1

3712

1560

4213

9296

5262

45.2

165.9

19.0

152.9 0.968 0.799

1.554

DAY 2

3880

1576

4061

9156

5207

46.6

163.6

17.9

154.4 0.938 0.743

1.547

DAY 3

4142

1582

4037

9174

5167

45.5

164.9

18.4

146.5 0.974 0.789

1.571

DAY 4

4103

1571

3933

9158

5146

45.0

164.3

18.4

146.4 0.969 0.813

1.564

DAY 5

4200

1608

4024

9334

5229

46.2

166.9

18.7

149.4 0.986 0.779

1.598

MEAN

4007

1579

4054

9223

5202

45.7

165.1

18.5

149.9 0.967 0.785

1.567

%RSD

5.1

1.1

2.5

0.9

0.9

1.5

0.8

2.2

2.4

1.8

3.4

1.3

CERTIFIED VALUES

4182 - 4348

1612 - 1684

3850 - 4130

9110 - 9330

5202 - 5304 47.8 - 50.6 172.7 - 178.5

19.52 - 20.04

145.4 - 156.6

1.04 - 1.10

0.783 - 0.841

1.667 - 1.747