AOAC SPSFAM Cannabis Concentrates SMPR v2.docx
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Table 2: Method performance requirements (part 1).
Requirement THC, THCA, CBDA, CBD, Individually Reported
Requirement (Additional, Desirable Cannabinoids (Table 1b), including CBN)
Parameter
Limit of Quantitation (LOQ) (% w/w)
≤ 0.3
≤ 0.3
Analytical Range (% w/w)
≤ 0.3 – ca. 100
≤ 0.3 – ca. 50
95 96 97 98 99
*Reported as individual cannabinoids
100 101 102 103 104 105 106
Table 3: Method performance requirements (part 2).
Ranges (% w/w)
Parameters
≤ 0.3 – 1
> 1 ‐ 10
> 10 – ca. 100
Recovery (% w/w)
95 – 105
97 ‐ 103
98 ‐ 102
% RSD r % RSD R
≤ 5
≤ 4
≤ 2
≤ 7
≤ 5
≤ 3
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