AOAC STANDARDS & METHODS ORIENTATION E-BOOK
9/10/2019
Guide to Method Format
• Title • Applicability (SMPR can guide) • Principle • Apparatus (SMPR can guide) • Reagents • Sample
Preparation/Analysis/Determination/Preparation of Standard Solutions (may have subsections)
• Calculation • Reference
Preparing a Candidate Method
Publishing a technique in a peer reviewed journal can be a start, but is not enough
Testing your method to ensure that all method parameters are characterized, accuracy determined and precision are required Analytical working ranges, recovery/accuracies, Forms of limits (LOD, LOQ, MDL, AMDL, etc…) Commodity matrices for which method applies Repeatability, robustness, reproducibility*) •*Reproducibility is required for Final Action consideration
Write the method into AOAC format and see if it can be followed as written.
Evaluate and Test the Method !!!
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