AOAC2016-03ERPRECOMMENDATION

2016.03 (Nov. 2017) - Chlor-02/04 Final Action Review FOR ERP USE ONLY DO NOT DISTRIBUTE

Summarized results of the full MLT set of samples can be found in Table 1 below.

≤ 2 %

≤ 4 %

Requirements (SMPR 2014.015)

Mean

RSD r (%)

RSD R (%)

HorRat (%)

Sample

n

Adult Nutritional Powder Low Fat

16 10 16 16 16 15 14 15 15 15 14 13 16 16 11 11 16 16 12 12 10 13 11 8

385.5 162.6 154.2 701.1 478.6 510.3 413.7 330.4 386.1 380.2 357.3 443.6 372.5 42.4

0.58 1.05 1.94 0.72 0.87 0.94 1.12 1.76 1.12 0.73 0.61 1.00 0.44 0.83 1.49 0.52 1.68 1.28 0.56 1.37 0.68 1.5 1.12

3.46 2.54 3.01 2.44 3.76 2.34 2.01 3.49 2.54 4.08 2.27 3.67 3.56 3.90 3.50 2.24 3.47 3.85 2.57 2.72 3.57 2.8 3.89

0.75 0.48 0.57 0.58 0.84 0.36 0.45 0.76 0.54 0.88 0.49 0.78 0.79 0.84 1.09 0.60 3.11 0.49 0.48 0.75 0.64 0.74 0.61 0.48

Adult Nutritional RTF High Fat

Adult Nutritional RTF High Protein

SRM 1849a

Toddler Formula Powder Milk Based

Infant Formula RTF Milk Based

Infant Formula Powder Soy Based Infant Formula Powder Milk Based Infant Formula Powder FOS/GOS Based Infant Formula Powder Part Hyd Soy Based Infant Formula Powder Part Hyd Milk Based

Infant Formula Powder Milk Based Child Formula Powder Milk Based

Infant Elemental Powder

Adult Nutritional RTF High Fat – Placebo

35.4 40.2 32.4 22.5

3.14*

7.21*

Adult Nutritional RTF High Protein – Placebo Child Formula Powder Milk Based – Placebo

12.4*

20.8*

Infant Formula RTF Milk Based – Placebo

Infant Elemental Powder – Placebo

358.9 375.5 562.2 169.5 711.6

IDF – Butter IDF- Cheese

IDF - Whey Protein Concentrate

IDF – Whole Milk Powder

IDF – Whole Milk

95.3

IDF – Whey Powder

9

281.3

0.74 _______ _______ _________

n = number of laboratories (after outliers removal) RSD r : relative standard deviation of repeatability RSD R : relative standard deviation of reproducibility

23

25