ISPAM Working Group Chair Presentation Book

SMPR Key Points:  Identification Method

Minimum  Acceptable   Results 90% POI § of  the pooled  data for all  target  compounds  and matrices

Target Test  Concentration

Parameter

Parameter Requirements

Minimum of 33 replicates  representing all target  compounds in Annex II and all 

100 ppm 

POI @ low 

concentration matrix types listed in Annex III,  spiked at or below the designated  low level target test conc.

y Validation

Minimum of 5 replicates per  matrix type spiked at 10x the  designated low level target test 

POI @ high  concentration 

10 x  low conc.

100% correct  analyses are  expected

conc.

e Laborator

Singl

Minimum of 5 replicates per  matrix type . 

POI @ zero  concentration

0 ppm

§ 95% confidence interval