Low Lactose ERP - Review Book

AOAC SMPR ERPs - 2019 METHOD REVIEW FORM

Submission Date

2019-08-31 09:08:23

Name

TOMASZ TUZIMSKI

E-mail

tomasz.tuzimski@umlub.pl

Organization

Medical University of Lublin, Poland

Title of Method

Quantitation of Six Common Food Sugars in Various Matrices by HPLC-MS

AOAC Candidate Method Number (e.g. ALN-01)

LAC-002

Applicable SMPR

AOAC SMPR 2018.009

I. Summary of the Method

The proposed method (LAC-002) entitled ‘Quantitation of Six Common Food Sugars in Various Matrices by HPLC-MS’ described Kai Liu, Ben Pointer is applicable for the detection and quantitation of the content of six common mono and disaccharides (fructose, galactose, glucose, sucrose, maltose, and lactose) in various food, infant formula, feed and pet food matrices. The developed method was evaluated following the definitions of Standard Method Performance Requirements (SMPRs®) for Lactose in Low-Lactose or Lactose-Free Milk, Milk Products, and Products Containing Dairy Ingredients (AOAC SMPR 2018.009) with respect to Limit of Detection (LOD) and the Limit of Quantitation (LOQ), Linearity, Repeatability, Reproducibility, Recovery.

II. Review of the Method Only 1. Does the applicability of the method support the applicability of the SMPR? If not, please explain what is missing. 2. Does the analytical technique(s) used in the method meet the SMPR? If not, please specify how it differs from what is stated in the SMPR. 3. Are the definitions specified in the SMPR used and applied appropriately in the method? If no, please indicate how the terms are used.

Generally: YES: The applicability of the method is adequate to the applicability of the SMPR.

YES: The analytical techniques in the method are adequate and meet the SMPR.

YES: Definitions, which are specified in the SMPR, were listed in the description, also were applied appropriately in the method.