MCPD-02 Reviewer Forms (July 19, 2018)

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Reviewer 9

Bound Glycidol in powder and liquid samples: 10 and 2  g/kg respectively

Accuracy/Recovery: Variable, in the range 72-125 %

Precision (RSD r

): 1.2 to 12 % (< 22 %)

Reproducibility (RSD R

): no comments.

System suitability: No concerns.



Were the recommendations/comments completed as requested by the ERP? Yes, although there is no agreement with concern to ERP recommendations No 15 and 24 (linearity has not been explicitly demonstrated for bound analytes) and No 18 (with relation to the impact of matrix types). However, the Author has provided two detailed answers.

Recommendation for First Action Official Methods SM status: I recommend that the ERP adopt this method for First Action Official Method SM status.

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