March 17, 2015-SP

3/17/2015

CALIBRATION/QC STANDARDS

CS 1 CS 2 CS 3 CS 4 CS 5 CS 6

0.001 0.002 0.005

0.01 0.05

0.1

In powder In liquid QC Std ug/g (ug/mL) MQL 0.01 0.001 QC-Low 0.025 0.0025 QC-Med 0 1 0 01 . .

QC-High 0.5

0.05

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MFA‐AOAC, 2015 

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STANDARD CURVE DATA (3 DAYS)

%Accuracy

WS1 WS2 WS3 WS4 WS5 WS6

Day-1 1 Day-2 1 Day-3 1 2 2

104

99.9

91.5 105.9 96.5 101.5

103.7 100.1 92.2 106.6 96.6 101.4

103

98.4

93.3 106.2 97.2 101.5

104 100 1 92 2 106 6 96 3 101 2 . . . . .

99

101.7 91.7 108.6

97

101.3

2

101.5 101.3 91.6 108.9 96.5

101

Compound name:MFA-2NPH Correlation coefficient: r=0.999479, r^2=0.998959 Calibration curve:0.949233 * x+ -0.0152233

Response type: InternalStd (Ref2 ),Area * ( ISConc. / ISArea ) Curve type:Linear,Origin:Exclude,Weighting:1/x,Axis trans:None

5.0

0.0

Residual

-5.0

Conc

80.0

60.0

40.0

Response

20.0

-0.0

Conc -0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100

Proprietaryand confidential — do not distribute © 2015 Abbott Laboratories

MFA‐AOAC, 2015 

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