OMB First to Final Action Recommendation Checklist 11-12-18

CHECKLIST FOR AOAC FINAL ACTION METHOD RECOMMENDATION

AOAC OMA 2014.09 Determination and Confirmation of Residues of 653 Multiclass Pesticides and Chemical Pollutants in Tea

OMB GUIDANCE FOR AOAC ERPS

Considered?

Comments

Method Applicability

Yes

Determination and Confirmation of Residues of 653 Multiclass Pesticides and Chemical Pollutants in Tea GC/MS, GC/MS/MS, and LC/MS/MS Completed prior to AOAC First Action All addressed prior to No reference materials available. Authors used two (2) internal standards for quantitation.

Safety Concerns

Yes No

Reference Materials

Single Laboratory Validation

Yes Yes

Pre-Collaborative

Reproducibility/Uncertainty and Probability of Detection

• J. AOAC Int., Volume 98, Number 5, September-October 2015, pp. 1428-1454(27) • J. AOAC Int., Volume 98, Number 5, September-October 2015, pp. 1428-1454(27) • J. AOAC Int. Volume 98, Number 5, September-October 2015, pp. 1428-1454(27)

Comparison to SMPR

No Yes

SMPR, not applicable. Discussed in ERP meeting

Feedback from Users of Method

ERP Recommendation to Repeal First Action Method

Not Applicable

DOCUMENTATION Safety Evaluation Reference Materials

Available?

Comments

Yes No Yes Yes Yes Yes No Yes Yes

Completed prior to AOAC First Action

No reference materials available. Authors used two (2) internal standards for quantitation.

SLV or PTMs

In manuscript Collaborative

Approved Validation Protocols

Statistics Review

Completed prior to AOAC First Action

Method Published in OMA

OMA 2014.09

Method Performance vs SMPR criteria

SMPR, not applicable. Discussed in ERP meeting

Feedback Information Additional Recognition(s)

AOAC Method of the Year Award

ERP Reports

Yes

September 2014; March 2017

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