OMB Meeting Book_9-11-14

Table 3

Precision - repeatability.

Nr. replicates (n) (Duplicates on 2-9 days)

Conc. Level (mcg/100g liquid)

Product

SPIFAN Code

Analyte

Conc. Level

REQUIREMENTS SMPR

RSDr

RSD iR

RSDr

RSD iR

Child Formula Powder Infant Elemental Powder

00411RF00 00402RF00 00415RF00 00407RF00

Vitamin B12 Vitamin B12 Vitamin B12 Vitamin B12 Vitamin B12 Vitamin B12 Vitamin B12 Vitamin B12 Vitamin B12 Vitamin B12 Vitamin B12 Vitamin B12 Vitamin B12

10

0.112

5.6

8.7

(mcg/100g liquid)

≤ Z % ≤ W %

6 8 4 8

ND

Vitamin B12 Vitamin B12 Vitamin B12 Vitamin B12

0.01

≤ 15

Adult Nutrional RTF, High Protein Adult Nutrition RTF, High Fat Infant Formula RTF, Milk Based

0.0259

13.2

0.2 0.5

≤ 7 ≤ 7 ≤ 7

ND

SPIFAN Blank Milk Form Vitamin B12

0.546 42.4 a 0.299 0.377 0.257 0.666 0.955 0.540 0.236 0.415 0.355

6.8

19.4

5

SRM 1849a

CLC10-b

18 12 12 12 12 12 12 12 12 12 12 12

3.3 4.7 3.5 3.5 2.8 2.4 4.1 3.5 3.6 2.3 2.2 2.8

3.7 5.4 9.6 5.9 4.9 2.9 5.0 6.1 6.2

Adult Nutritional Powder Milk Protein Based

11750017V3 1172572116 117257651Z 00394RF00 00412RF00 00403RF00 D04HTCVV

Infant Formula Powder Partially Hydrolyzed Milk Based Infant Formula Powder Partially Hydrolyzed Soy Based

Adult Nutritional Powder Low Fat

Child Formula Powder Infant Elemental Powder

Infant Formula Powder Milk Based Infant Formula Powder Soy Based Infant Formula RTF Milk Based Adult Nutrional RTF High Protein

E29JVLV

SPIFAN Control Milk Form Vitamin B12

14.7

00414RF00 00406RF00

Vitamin B12 Vitamin B12

1.13 1.65

3.3 6.9

Adult Nutrition RTF High Fat

Global Mean %

4.3

7.3

a. Results reported as mg/kg powder since no standard reconstitution rate available.

SPIFAN ERP X Checklist v 1.0