OMB Meeting Book_9-11-14

Table 4

Precision - reproducibility

Conc. Level (mcg/100g RTF)

Product

REQUIREMENTS SMPR Conc. Level

SPIFAN Code

Analyte

Nr. replicates (n)

RSD R

RSD R

0.0437 a

SRM 1849a

CLC10-b

Vitamin B12 Vitamin B12 Vitamin B12 Vitamin B12 Vitamin B12 Vitamin B12 Vitamin B12 Vitamin B12 Vitamin B12

20 20 22 20 20 16 18 18 20 18 20 14

8.8

mcg/100g RTF

≤ Z %

Adult Nutritional Powder Milk Protein Based

11750017V3 1172572116 117257651Z 00394RF00 00412RF00 00403RF00 D04HTCVV

0.300 0.373

13.8 18.6 19.5

Vitamin B12

0.3-5.0

11

Infant Formula Powder Partially Hydrolyzed Milk Based Infant Formula Powder Partially Hydrolyzed Soy Based

0.25

Adult Nutritional Powder Low Fat

0.636 0.967 0.543 0.227 0.428 0.272 1.08 1.48 b

9.2 3.5

Child Formula Powder Infant Elemental Powder

11.1

Infant Formula Powder Milk Based Infant Formula Powder Soy Based Infant Formula RTF Milk Based Adult Nutrional RTF High Protein

8.9 7.1

E29JVLV

SPIFAN Control Milk Form Vitamin B12

15.7 17.5

00414RF00

Vitamin B12 Vitamin B12

Adult Nutrition RTF High Fat

00406RF00

11.5

a Results in mg/kg pwd b Includes single determinations for 4 laboratories because of mislabeled product cans.

Global Mean %

12.1

SPIFAN ERP Checklist v 1.0