OMB Meeting Book_9-11-14

Table 3

Precision - repeatability.

Nr. replicates (n) (Duplicates on 6-7 days)

Conc. Level (mg/100g liquid)

Product

SPIFAN Code

Analyte

Conc. Level

REQUIREMENTS SMPR

RSDr 2.00 2.95 2.02 2.22 3.06 2.32 2.17 3.48 1.47 3.05 2.46 1.89 5.05 4.69 4.00 3.36 2.40 4.43 1.96 2.76 1.80 1.63 2.07

RSD iR

RSDr

RSD iR

415.2 a

2.29 5.32 3.34 2.26 4.32 2.90 2.72 3.64 1.81 3.92 3.22 2.99 7.30 4.69 6.21 4.33 3.60 4.77 2.24 4.98 2.65 2.17 2.12

SRM 1849a

CLC10-b

Myo-inositol, Free Myo-inositol, Free Myo-inositol, Free Myo-inositol, Free Myo-inositol, Free Myo-inositol, Free Myo-inositol, Free Myo-inositol, Free Myo-inositol, Free Myo-inositol, Free Myo-inositol, Free Myo-inositol, Free

14 14 14 14 14 14 14 14 14 12 12 12 12 12 12 12 12 12 12 12 12 12 12

(mg/100g liquid)

≤ Z % ≤ W %

3.38

Infant Formula Powder Partially Hydrolyzed Milk Based Infant Formula Powder Partially Hydrolyzed Soy Based

1172572116 117257651Z 00412RF00 00403RF00 D04HTCVV

myo-inositol myo-inositol myo-inositol

2

≤ 5 ≤ 5 ≤ 5

3.099

20 68

5.04

Child Formula Powder Infant Elemental Powder

4.847 4.213 4.194

Infant Formula Powder Milk Based Infant Formula Powder Soy Based infant Formula RTF Milk Based Infant Formula RTF, Milk Based Placebo Adult Nutritional RTF High Protein, Spiked Child Formula Powder Placebo, Spiked

E29JVLV

SPIFAN Control Milk Form SPIFAN Blank Milk Form

7.19 3.17 61.4 1.94 1.74

00414RF00 00411RF00 00402RF00

Infant Elemental Powder Placebo

10.62 a

SRM 1849a

CLC10-b

Myo-inositol, from phosphatidylinositol Myo-inositol, from phosphatidylinositol Myo-inositol, from phosphatidylinositol Myo-inositol, from phosphatidylinositol Myo-inositol, from phosphatidylinositol Myo-inositol, from phosphatidylinositol

Adult Nutritional Powder Milk Protein Based

11750017V3 1172572116 117257651Z

1.43

Infant Formula Powder Partially Hydrolyzed Milk Based Infant Formula Powder Partially Hydrolyzed Soy Based

0.244 1.976 2.478 0.443

Infant Formula Powder Soy Based

E29JVLV

Child Formula Powder

00412RF00

425.8 a

SRM 1849a

CLC10-b

Myo-inositol, Total Myo-inositol, Total Myo-inositol, Total Myo-inositol, Total Myo-inositol, Total

Infant Formula Powder Partially Hydrolyzed Milk Based Infant Formula Powder Partially Hydrolyzed Soy Based

1172572116 117257651Z

3.63 5.08 6.67 5.48

Infant Formula Powder Soy Based

E29JVLV

Child Formula Powder

00412RF00

Global Mean %

2.7

3.6

Results reported as mg/kg powder since no standard reconstitution rate available

SPIFAN ERP X Checklist v 1.0