OMB Meeting Book_9-11-14

Table 4

Precision - reproducibility

Conc. Level (mg/100g RTF)

Product

REQUIREMENTS SMPR Conc. Level

SPIFAN Code

Analyte

Nr. replicates (n)

RSD R

RSD R

412 a 3.83 3.11 5.05 5.13 4.23 4.22

SRM 1849a

CLC10-b

Myo-inositol, Free Myo-inositol, Free Myo-inositol, Free Myo-inositol, Free Myo-inositol, Free Myo-inositol, Free Myo-inositol, Free Myo-inositol, Free Myo-inositol, Free

22 18 22 18 20 16 22 18 20 18 20 20 20 20 18 20 18 18 20 16 20 18 18 16 20 16 18

2.8 2.3

mg/100g RTF ≤ Z %

Infant Formula Powder Partially Hydrolyzed Milk Based Infant Formula Powder Partially Hydrolyzed Soy Based

1172572116 117257651Z 00412RF00 00403RF00 D04HTCVV

Myo-inositol

2.0-68.0

8

12.6

Child Formula Powder Infant Elemental Powder

2.2 5.4 2.6 7.3 2.6 2.9

Infant Formula Powder Milk Based Infant Formula Powder Soy Based infant Formula RTF Milk Based Infant Formula RTF, Milk Based Placebo

E29JVLV

SPIFAN CONTROL Milk Form SPIFAN BLANK Milk Form

7.2

3.17

9.26 a 0.214

SRM 1849a

CLC10-b

Myo-inositol, Phosphatidylinositol Myo-inositol, Phosphatidylinositol Myo-inositol, Phosphatidylinositol Myo-inositol, Phosphatidylinositol Myo-inositol, Phosphatidylinositol Myo-inositol, Phosphatidylinositol Myo-inositol, Phosphatidylinositol

25.0 26.4 21.1 25.8 25.9 23.2 25.2 26.9 0.0

Infant Formula Powder Partially Hydrolyzed Milk Based Infant Formula Powder Partially Hydrolyzed Soy Based

1172572116 117257651Z 00412RF00 00403RF00 D04HTCVV

1.64

Child Formula Powder Infant Elemental Powder

0.328

0

Infant Formula Powder Milk Based Infant Formula Powder Soy Based infant Formula RTF Milk Based Infant Formula RTF, Milk Based Placebo

0.667

E29JVLV

2.1

SPIFAN CONTROL Milk Form Myo-inositol, Phosphatidylinositol SPIFAN BLANK Milk Form Myo-inositol, Phosphatidylinositol

0.348 0.305

422 a 4.04 4.71 5.42 5.11 4.94 6.27 7.53 3.46

SRM 1849a

CLC10-b

Myo-inositol, Total Myo-inositol, Total Myo-inositol, Total Myo-inositol, Total Myo-inositol, Total Myo-inositol, Total Myo-inositol, Total Myo-inositol, Total Myo-inositol, Total

2.8 3.1 7.6 5.2 5.6 6.1 7.1 2.7 3.7

Infant Formula Powder Partially Hydrolyzed Milk Based Infant Formula Powder Partially Hydrolyzed Soy Based

1172572116 117257651Z 00412RF00 00403RF00 D04HTCVV

Child Formula Powder Infant Elemental Powder

Infant Formula Powder Milk Based Infant Formula Powder Soy Based Infant Formula RTF Milk Based Infant Formula RTF, Milk Based Placebo

E29JVLV

SPIFAN CONTROL Milk Form SPIFAN BLANK Milk Form

a Results in mg/kg pwd

Global Mean %

10.5

SPIFAN ERP Checklist v 1.0