OMB Meeting Book_9-11-14

Table 3: Homogeneity data for starch-based infant formula test sample

Sample ID: Sample 2 S-1111/S-2222 Analyte CMP

UMP

GMP

IMP

AMP

(mg hg -1 )

(mg hg -1 )

(mg hg -1 )

(mg hg -1 )

(mg hg -1 )

Replicate

Bag-1

Bag-2

Bag-1

Bag-2

Bag-1

Bag-2

Bag-1

Bag-2

Bag-1

Bag-2

1 2

10.94 10.93

10.95 11.10

3.80 3.77

4.04 4.04

1.64 1.62

1.64 1.67

1.59 1.61

1.61 1.61

3.42 3.42

3.50 3.55

3

10.90

11.07

3.80

3.98

1.66

1.69

1.57

1.59

3.46

3.55

4

10.98

10.77

3.93

3.75

1.63

1.58

1.58

1.57

3.46

3.36

5

11.09

11.03

3.95

3.70

1.71

1.66

1.60

1.61

3.55

3.47

Table 4: Homogeneity analysis for starch-based infant formula test sample

Sample ID: Sample 2 S-1111/S-2222 Analyte CMP

UMP

GMP

IMP

AMP

(mg hg -1 )

(mg hg -1 )

(mg hg -1 )

(mg hg -1 )

(mg hg -1 )

Item

Bag-1

Bag-2

Bag-1

Bag-2

Bag-1

Bag-2

Bag-1

Bag-2

Bag-1

Bag-2

Mean

10.97 0.074

10.98 0.132

3.85

3.90

1.65

1.65

1.59

1.60

3.46

3.49

S r

0.083

0.164

0.036

0.042

0.016

0.018

0.053

0.078

RSD r n (df)

0.7

1.2

2.2

4.2

2.2

2.6

1.0

1.1

1.5

2.2

5 (4)

5 (4)

5 (4)

5 (4)

5 (4)

5 (4)

5 (4)

5 (4)

5 (4)

5 (4)

t calc T tab

0.22 2.78

0.47 2.78

0.20 2.78

1.37 2.78

0.51 2.78

p-value

0.84

0.66

0.85

0.24

0.64