OMB Meeting Book_9-11-14

Table 5: Homogeneity data for hydrolysate-based infant formula test sample

Sample ID: Sample 3 X-8281/D-5352 Analyte CMP

UMP

GMP

IMP

AMP

(mg hg -1 )

(mg hg -1 )

(mg hg -1 )

(mg hg -1 )

(mg hg -1 )

Replicate

Bag-1

Bag-2

Bag-1

Bag-2

Bag-1

Bag-2

Bag-1

Bag-2

Bag-1

Bag-2

1 2

9.06 9.19

8.30 8.93

3.51 3.58

4.05 3.63

1.48 1.34

1.61 1.33

2.38 2.42

2.26 2.38

4.44 4.51

3.94 4.32

3

9.22

8.24

3.47

3.96

1.37

1.36

2.44

2.26

4.54

3.87

4

8.89

9.01

3.69

3.56

1.24

1.28

2.36

2.38

4.30

4.34

5

9.05

9.05

3.47

3.38

1.31

1.60

2.39

2.39

4.41

4.43

Table 6: Homogeneity analysis for hydrolysate-based infant formula test sample

Sample ID: Sample 3 X-8281/D-5352 Analyte CMP

UMP

GMP

IMP

AMP

(mg hg -1 )

(mg hg -1 )

(mg hg -1 )

(mg hg -1 )

(mg hg -1 )

Item

Bag-1

Bag-2

Bag-1

Bag-2

Bag-1

Bag-2

Bag-1

Bag-2

Bag-1

Bag-2

Mean

9.08

8.71

3.54

3.72

1.35

1.44

2.40

2.33

4.44

4.18

S r

0.131

0.401

0.093

0.281

0.088

0.157

0.032

0.068

0.094

0.256

RSD r n (df)

1.4

4.6

2.6

7.6

6.5

10.9

1.3

2.9

2.1

6.1

5 (4)

5 (4)

5 (4)

5 (4)

5 (4)

5 (4)

5 (4)

5 (4)

5 (4)

5 (4)

t calc T tab

1.76 2.78

1.20 2.78

1.55 2.78

1.70 2.78

1.84 2.78

p-value

0.15

0.30

0.19

0.16

0.14