OMB Meeting Book_9-11-14

Repeatability relative standard deviation Reproducibility relative standard deviation

RSD(r) RSD(R)

16.60 22.61

3.73 7.81 0.59

4.42

49.80 49.80

17.25 26.74

16.00

HORRAT value

1.56

1.25

2.80

1.25

Outliers

Tocopherol Acetate Total number of laboratories Total number of replicates Overall mean of all data (grand mean) Repeatability standard deviation Reproducibility standard deviation Repeatability relative standard deviation Reproducibility relative standard deviation Tocopherol Total number of laboratories Total number of replicates Overall mean of all data (grand mean) Repeatability standard deviation Reproducibility standard deviation Repeatability relative standard deviation Reproducibility relative standard deviation HORRAT value Outliers

15 30

15 30

15 30

15 30

15 30

p

Sum(n(L)) XBARBAR

6.06

4.61

1.48

12.34

1.80

s(r) s(R)

0.1489 0.3732

0.1438 0.3048

0.2350 0.2670

0.4722 1.7616

0.0657 0.2025

RSD(r) RSD(R)

2.46 6.16 0.70

3.12 6.61 0.73

15.88 18.04

3.83

3.65

14.28

11.25

0.60

1.81

1.07

15 30

15 30

15 30

15 30

15 30

p

Sum(n(L)) XBARBAR

2.59

6.28

0.34

0.60

0.47

s(r) s(R)

0.2027 0.4661

0.3773 1.1742

0.1489 0.1658

0.0225 0.1197

0.1038 0.1421

RSD(r) RSD(R)

7.82

6.00

43.66 48.62

3.72

22.02 30.12

17.99

18.68

19.81

HORRAT value

1.81

2.14

3.64

1.60

2.36

Outliers

Total E Total number of laboratories Total number of replicates Overall mean of all data (grand mean) Repeatability standard deviation Reproducibility standard deviation Repeatability relative standard deviation

15 30

15 30

15 30

15 30

15 30

p

Sum(n(L)) XBARBAR

5.98

7.73

1.82

12.94

2.27

s(r) s(R)

0.1955 0.3886

0.3524 0.7946

0.2339 0.3186

0.4804 1.6837

0.1240 0.2307

RSD(r)

3.27

4.56

12.85

3.71

5.46