OMB Meeting Book - Jan. 11, 2018

110 H ALBMAYR -J ECH ET AL . : J OURNAL OF AOAC I NTERNATIONAL V OL . 98, N O . 1, 2015

Lab Sample 1 Sample 2 Sample 3 Sample 4 Sample 5 Sample 6 Sample 7 Sample 8 Sample 9 Sample 10 Sample 11 Sample 12 A 0, 7 0, 3 14, 1 18, 3 21, 4 23, 1 107, 5 115, 5 –1, 1 0, 1 4, 6 4, 7 12, 4 10, 1 61, 0 59, 5 2, 5 3, 2 12, 0 13, 7 26, 5 24, 9 92, 1 109, 9 D 1, 1 3, 6 18, 5 17, 6 39, 8 53, 9 150, 5 162, 8 0, 9 0, 3 9, 3 7, 1 16, 2 17, 3 121.4 b 120.7 b 5, 8 3, 7 16, 8 18, 2 45, 0 41, 6 154, 5 159, 7 E 0, 4 0, 6 17, 7 14, 7 19, 1 48, 6 149, 1 177, 6 0, 9 –1, 2 6, 7 6, 1 12, 6 15, 9 79, 7 78, 5 0, 3 0, 5 11, 8 11, 0 17, 8 19, 9 102, 0 104, 9 F 0, 2 0, 4 11, 4 15, 6 19, 2 10, 2 58, 1 71, 2 0, 0 –2, 1 5, 3 5, 4 12, 1 10, 9 71, 2 62, 3 6, 7 2, 0 12, 0 9, 1 18, 8 18, 4 86, 7 79, 3 G 1, 2 0, 8 9, 1 14, 6 27, 3 26, 3 76, 7 70, 4 0, 5 –0, 9 7, 2 4, 9 12, 0 11, 6 52, 2 55, 4 4, 0 3, 0 13, 5 13, 8 22, 2 27, 0 103, 6 86, 5 H –0, 2 –0, 3 7, 7 7, 2 12, 6 14, 1 64, 2 60, 8 0, 7 0, 3 5, 3 6, 1 11, 9 13, 1 60, 4 59, 9 0, 7 0, 6 9, 1 8, 9 17, 3 16, 4 73, 8 66, 3 I 2, 0 2, 8 15, 6 12, 9 22, 7 19, 0 81, 5 78, 0 –1, 3 1, 9 3, 9 7, 1 10, 1 11, 7 51, 1 39, 0 5, 5 4, 9 15, 2 15, 0 39, 3 26, 2 65, 8 100, 4 K 6, 7 5, 6 15, 7 15, 5 38, 7 29, 9 85, 6 76, 0 0, 4 –0, 8 4, 3 4, 5 8, 9 11, 2 40, 1 39, 4 13.5 b 14.6 b 26, 0 23, 3 36, 4 36, 8 158, 4 114, 6 L 8.9 c 0.5 c 22, 0 17, 5 38, 3 56, 8 120, 5 143, 2 2, 9 –1, 7 9, 8 9, 1 12, 9 15, 1 66, 2 75, 4 3, 0 4, 7 13, 4 17, 2 34, 9 21, 4 118, 5 175, 7 M 3, 9 3, 5 18, 5 17, 7 20, 3 38, 9 99, 6 81, 4 0, 6 –0, 4 5, 3 7, 6 15, 5 13, 6 70, 3 78, 8 6, 9 11, 1 21, 3 19, 7 16, 9 21, 1 154, 6 90, 3 N 1, 7 4, 7 9, 7 12, 7 18, 9 15, 0 145, 0 111, 6 0, 1 0, 9 4, 5 3,8 9,6 9,5 45,5 52,0 4,8 10,9 11,1 10,4 20,6 23,8 102,1 90,5 O 1,3 1,9 15, 9 7, 4 26, 2 36, 2 124, 5 95, 6 0.3 c 1.5 c 6, 8 4, 9 18, 7 13, 9 73.6 c 108.7 c 4, 4 1, 6 19, 3 15, 3 26, 7 27, 5 144, 8 142, 8 U 2, 5 2, 8 16, 4 17, 7 26, 5 29, 0 97, 0 109, 4 –2.28 b –2.74 b 11, 0 7, 8 17, 3 17, 9 76, 9 91, 2 4, 6 8, 4 19, 6 22, 7 33, 4 41, 4 139, 6 141, 3 a *OXWHQ IUHH ULFH ÀRXU ULFH ÀRXU PJ JOXWHQ NJ ULFH ÀRXU PJ JOXWHQ NJ ULFH ÀRXU PJ JOXWHQ NJ JOXWHQ IUHH FKRFRODWH FDNH FKRFRODWH FDNH PJ JOXWHQ NJ FKRFRODWH FDNH PJ gluten/kg; 8 = chocolate cake 100 mg gluten/kg; 9 = crisp bread 4.5 mg gluten/kg; 10 = crisp bread 15 mg gluten/kg; 11 = crisp bread 24 mg gluten/kg; and 12 = crisp bread 102 mg gluten/kg. b Grubbs outlier. c Cochran outlier.

Sample ID a

P –0, 6 1, 1 7, 7 11, 1 14, 5 14, 2 74, 1 74, 5 0, 5 0, 1 7, 5 7, 0 13, 7 12, 7 71, 3 66, 1 6, 6 3, 5 12, 0 16, 4 22, 9 18, 7 75, 7 70, 8 Q 0, 3 0, 6 12, 6 10, 3 18, 9 13, 7 114, 9 108, 1 –0, 7 –1, 2 5, 3 6, 6 12, 1 13, 2 67, 7 69, 7 2, 5 2, 3 12, 6 11, 3 23, 2 20, 3 112, 9 99, 8 R 3, 3 3, 6 11, 3 15, 2 25, 2 32, 2 139, 4 93, 1 0, 3 0, 1 6, 5 6, 4 14, 1 12, 8 72, 6 70, 5 6, 4 6, 6 19, 3 19, 1 46, 0 38, 9 178, 5 152, 9 S 0, 8 1, 0 9, 9 7, 6 31, 9 17, 9 92, 3 58, 7 0, 9 0, 3 5, 7 3, 8 10, 8 10, 3 44, 1 55, 1 1, 3 2, 0 12, 4 11, 9 28, 6 18, 2 109, 2 60, 7 T –1, 1 –1, 4 10, 1 9, 3 21, 0 22, 7 95, 2 77, 8 0, 2 0, 1 6, 6 4, 6 14, 2 14, 2 71, 8 76, 9 1, 7 1, 1 9, 8 10, 6 19, 8 20, 0 109, 7 129, 0

7DEOH ,QGLYLGXDO UHVXOWV IURP LQWHUODERUDWRU\ VWXG\ IRU JOXWHQ E\ $JUD4XDQW *OXWHQ * 6DQGZLFK (/,6$ UHVXOWV DUH VWDWHG DV PJ JOXWHQ NJ 2XWOLHUV GHWHUPLQHG ZLWK &RFKUDQ DQG WKH *UXEEV WHVW DUH PDUNHG LQ EROG IRQW DQG KLJKOLJKWHG LQ JUH\ /DERUDWRU\ % GLG QRW UHWXUQ D UHVXOW VKHHW LQ WLPH 5HVXOW VKHHWV RI ODERUDWRULHV & DQG - FRXOG QRW be used