Review Team (February 2016)
Bio-03 (February 2016) FOR ERP USE ONLY DO NOT DISTRIBUTE
Table 2. Accuracy – spike recovery.
Spike Recovery
Level 2 (~150% for placebo, ~100% for fortified)
Nr. replicates (n)
Level 1 (~50%)
Native level (mcg/100g reconstituted)
Product
SPIFAN Code
Avg (%) n=3
RSD (%)
Avg (%) n=3
RSD (%)
Child Formula Powder, placebo Adult Nutritional RTF High Protein, placebo Adult Nutritional RTF High Fat, placebo Infant Formula Powder Partially Hydrolyzed Soy Based
00847RF00
6
Not detected
103
3.2
105
1.5
00821RF00
6
Not detected
102
1.6
103
1.5
00820RF00
6
Not detected
102
2.2
104
1.7
410457651Z
6
4.43
105
4.2
101
4.2
Adult Nutritional Powder Low Fat
00859RF00 00866RF00
6 6
31.9 21.6
111 109
2.9 2.8
102 104
1.8 1.7
Child Formula Powder
Infant Elemental Powder
00795RF00
6
10.7
106
2.8
95.1
3.0
Infant Formula Powder FOS/GOS Based Infant Formula Powder Milk Based Adult Nutritional RTF High Protein Adult Nutritional RTF High Fat
50350017W1
6
1.66
105
6.4
99.9
7.2
K16NTAV
6
5.11
104
6.1
103
4.6
00730RF00
6
56.8
109
1.6
102
0.8
00729RF00
6
76.2
109
2.4
101
0.7
Table 3. Accuracy – recovery of SRM 1849a.
SRM Product
Code
Reference value
Measured value
Recovery vs CoA
(mg/kg powder)
(mg/kg powder)
%
1.969 2.067 2.081 2.023 2.047 1.971 2.013 1.987 1.995
99
104 105 102 103 101 100 100 99
1849a
CLC-10b
1.99
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