Review Team (February 2016)

Bio-03 (February 2016) FOR ERP USE ONLY DO NOT DISTRIBUTE

Table 2

Accuracy - Spike Recovery

Spike Recovery

Not detected Not detected Not detected Native level (mcg/100g liquid)

Level 1 (~50%)

Level 2 (~150% for placebo, ~100% for fortified)

Product

SPIFAN Code

Analyte

Nr. replicates (n)

Avg (%) n=3

RSD %

Avg (%) n=3

RSD (%)

Child Formula Powder, placebo

00847RF00 00821RF00 00820RF00 410457651Z 00859RF00 00866RF00 00795RF00 50350017W1 K16NTAV 00730RF00 00729RF00

Biotin Biotin Biotin Biotin Biotin Biotin Biotin Biotin Biotin Biotin Biotin

6 6 6 6 6 6 6 6 6 6 6

103 102 102 105 111 109 106 105 104 109 109

3.2 1.6 2.2 4.2 2.9 2.8 2.8 6.4 6.1 1.6 2.4

105 103 104 101 102 104 95.1 99.9 103 102 101

1.5 1.5 1.7 4.2 1.8 1.7 3.0 7.2 4.6 0.8 0.7

Adult Nutritional RTF High Protein, placebo Adult Nutritional RTF High Fat, placebo

Infant Formula Powder Partially Hydrolyzed Soy Based

4.43 31.9 21.6 10.7 1.66 5.11 56.8 76.2

Adult Nutritional Powder Low Fat

Child Formula Powder Infant Elemental Powder

Infant Formula Powder FOS/GOS Based Infant Formula Powder Milk Based Adult Nutritional RTF High Protein

Adult Nutritional RTF High Fat

Global Mean %

106

3.3

102

2.6

SPIFAN ERP Checklist v1.0