Review Team (February 2016)

Amino-03 (February 2016) FOR ERP USE ONLY DO NOT DISTRIBUTE

===================================================================== Calibration Curves =====================================================================

Histidine at exp. RT: 2.305 DAD1 A, Sig=260,4 Ref=off Correlation: 0.99947 Residual Std. Dev.: 0.03194 Formula: y = mx + b m: 1.13672 b: -2.23043e-2 x: Amount y: Area

Area Ratio

0 0.25 0.5 0.75 1 1.25 1.5 1.75 2 2.25 0 0.25 0.5 0.75 1 1.25 1.5 1.75 2 2.25 0 0.25 0.5 0.75 1 1.25 1.5 1.75 0 0.25 0.5 0.75 1 1.25 1.5 1.75 2

5

4

3

2

1

0

1

2

Amount Ratio

Taurine at exp. RT: 3.078 DAD1 A, Sig=260,4 Ref=off Correlation: 0.99947 Residual Std. Dev.: 0.03174 Formula: y = mx + b m: 1.13459 b: -1.73419e-2 x: Amount y: Area

Area Ratio

5

4

3

2

1

0

1

2

Amount Ratio

Serine at exp. RT: 3.361 DAD1 A, Sig=260,4 Ref=off Correlation: 0.99984 Residual Std. Dev.: 0.01523 Formula: y = mx + b

Area Ratio

5

4

m: 9.77128e-1 b: 6.61918e-3 x: Amount y: Area

3

2

1

0

1

2

Amount Ratio

Argenine at exp. RT: 3.521 DAD1 A, Sig=260,4 Ref=off Correlation: 0.99979 Residual Std. Dev.: 0.01903 Formula: y = mx + b m: 1.07183 b: -1.13097e-2 x: Amount y: Area

Area Ratio

5

4

3

2

1

0

1

2

Amount Ratio

UPLC-DAD 7/31/2015 5:54:40 PM Vikas Kanase

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