Review Team (February 2016)

Amino-03 (February 2016) FOR ERP USE ONLY DO NOT DISTRIBUTE

RT Sig Lvl Amount Area Rsp.Factor Ref ISTD # Compound [mg/kg] -------|-|--|----------|----------|----------|---|---|-|------------------- 3.231 1 7 1.00000e-1 5.15000 1.94175e-2 No No Tryptophan

1 5.00000e-1 17.71609 2.82229e-2 2 1.00000 30.97373 3.22854e-2 3 5.00000 156.94293 3.18587e-2 4 10.00000 298.09192 3.35467e-2 5 20.00000 609.94220 3.27900e-2 6 50.00000 1481.52478 3.37490e-2

--------------------------------------------------------------------- --------------------------------------------------------------------- Peak Sum Table --------------------------------------------------------------------- ***No Entries in table*** --------------------------------------------------------------------- ===================================================================== Calibration Curves =====================================================================

Tryptophan at exp. RT: 3.231 FLD1 A, Ex=280, Em=356 Correlation: 0.99988 Residual Std. Dev.: 8.02455 Formula: y = mx + b m: 29.84370 b: 2.26817 x: Amount y: Area Calibration Level Weights: Level 7 : 1

Area

1000 1200 1400

6

0 200 400 600 800

5

4

3

712

0

20

40

Amount[mg/kg]

Level 1 : 0.2 Level 2 : 0.1 Level 3 : 0.02 Level 4 : 0.01 Level 5 : 0.005 Level 6 : 0.002

=====================================================================

UPLC-DAD 2/2/2016 7:59:54 PM

Page 2 of 2