Review Team (February 2016)

Fonterra Co-operative Group VitD-18 (February 2016) FOR ERP USE ONLY DO NOT DISTRIBUTE

Appendix B: Data—Precision Table B1: Data vitamin D 3

precision experiment 1

Vitamin D 3 Duplicate 1

Sample

Units

Duplicate 2

μg hg -1 μg hg -1 μg hg -1 μg hg -1 μg hg -1 μg hg -1 μg hg -1 μg hg -1 μg hg -1 μg hg -1 μg hg -1 μg hg -1

In-House Reference

10.0

9.9 9.4 9.1 7.9 8.4 8.1 3.3 7.9 7.7 6.8 9.7 9.4 6.5 9.4

SRM1849a

9.8 9.0 7.9 8.3 7.9 3.3 7.9 7.8 6.6 9.4 6.5 9.6

IF Powder Part. Hydrolysed Milk-Based IF Powder Part. Hydrolysed Soy-Based Toddler Formula Powder Milk-Based

IF Powder Milk-Based AN Powder Low Fat Child Formula Powder Infant Elemental Powder IF Powder FOS/GOS-Based

IF Powder Milk-Based IF Powder Soy-Based IF RTF Milk-Based AN RTF High Protein

10.1

μg L -1 μg L -1 μg L -1

AN RTF High Fat

12.1

13.5

Table B2: Data vitamin D 3

precision experiment 2

Vitamin D 3 Duplicate 1

Sample

Units

Duplicate 2

μg hg -1 μg hg -1 μg hg -1 μg hg -1 μg hg -1 μg hg -1 μg hg -1 μg hg -1 μg hg -1 μg hg -1 μg hg -1 μg hg -1

In-House Reference

10.3

10.3

SRM1849a

9.4

9.9

IF Powder Part. Hydrolysed Milk-Based IF Powder Part. Hydrolysed Soy-Based Toddler Formula Powder Milk-Based

10.2

10.5

9.1 8.5 8.0 3.3 7.7 7.8 6.7 9.6 9.4 6.5 9.5

8.9 8.2 8.4 3.3 7.7 6.7 9.7 9.2 6.5 9.4 7

IF Powder Milk-Based AN Powder Low Fat Child Formula Powder Infant Elemental Powder IF Powder FOS/GOS-Based

IF Powder Milk-Based IF Powder Soy-Based IF RTF Milk-Based AN RTF High Protein

μg L -1 μg L -1 μg L -1

AN RTF High Fat

12.2

11.9

Page 20