Review Team (February 2016)

Fonterra Co-operative Group VitD-18 (February 2016) FOR ERP USE ONLY DO NOT DISTRIBUTE

Appendix D: Data—Recovery Table D1: Data vitamin D 2

100% recovery experiment 1

(μg hg -1 )

Vitamin D 2

Recovery (%)

Sample

Units

Unspiked sample

Spiked sample

Spike

μg hg -1 μg hg -1

Child Formula Powder Infant Elemental Powder

0.0 0.1 0.0 0.4 0.1

7.0 6.8

6.9 6.9

101.3

98.0 98.2

μg L -1 μg L -1 μg L -1

Adult Nutritional RTF High Protein Adult Nutritional RTF High Fat Infant Formula RTF, Milk-Based

13.6 14.3 13.5

13.8 13.8 13.8

100.9

97.1

Table D2: Data vitamin D 2

50% recovery experiment 1

(μg hg -1 )

Vitamin D 2

Recovery (%)

Sample

Units

Unspiked sample

Spiked sample

Spike

μg hg -1 μg hg -1

Child Formula Powder Infant Elemental Powder

0.0 0.1 0.0 0.0 0.1

3.3 3.4 6.8 6.6 6.6

3.5 3.5 6.9 6.9 6.9

94.3 95.4 97.8 95.3 94.2

μg L -1 μg L -1 μg L -1

Adult Nutritional RTF High Protein Adult Nutritional RTF High Fat Infant Formula RTF, Milk-Based

Table D3: Data vitamin D 2

100% recovery experiment 2

(μg hg -1 )

Vitamin D 2

Recovery (%)

Sample

Units

Unspiked sample

Spiked sample

Spike

μg hg -1 μg hg -1

Child Formula Powder Infant Elemental Powder

0.0 0.1 0.0 0.1 0.1

7.0 6.7

6.9 6.9

101.1

96.3 99.6 99.1 99.3

μg L -1 μg L -1 μg L -1

Adult Nutritional RTF High Protein Adult Nutritional RTF High Fat Infant Formula RTF, Milk-Based

13.8 13.8 13.8

13.9 13.9 13.9

Table D4: Data vitamin D 2

50% recovery experiment 2

(μg hg -1 )

Vitamin D 2

Recovery (%)

Sample

Units

Unspiked sample

Spiked sample

Spike

μg hg -1 μg hg -1

Child Formula Powder Infant Elemental Powder

0.0 0.1 0.0 0.1 0.1

3.2 3.4 6.6 6.7 6.8

3.3 3.3 6.6 6.6 6.6

94.7 99.8 99.2

μg L -1 μg L -1 μg L -1

Adult Nutritional RTF High Protein Adult Nutritional RTF High Fat Infant Formula RTF, Milk-Based

100.4 101.9

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