Review Team (February 2016)

Fonterra Co-operative Group VitD-18 (February 2016) FOR ERP USE ONLY DO NOT DISTRIBUTE

Table D5: Data vitamin D 2

100% recovery experiment 3

(μg hg -1 )

Vitamin D 2

Recovery (%)

Sample

Units

Unspiked sample

Spiked sample

Spike

μg hg -1 μg hg -1

Child Formula Powder Infant Elemental Powder

0.1 0.1 0.0 0.0 0.1

7.3 7.2

7.2 7.2

100.7

98.3 99.1 96.0 94.8

μg L -1 μg L -1 μg L -1

Adult Nutritional RTF High Protein Adult Nutritional RTF High Fat Infant Formula RTF, Milk-Based

14.3 13.8 13.8

14.4 14.4 14.4

Table D6: Data vitamin D 2

50% recovery experiment 3

(μg hg -1 )

Vitamin D 2

Recovery (%)

Sample

Units

Unspiked sample

Spiked sample

Spike

μg hg -1 μg hg -1

Child Formula Powder Infant Elemental Powder

0.0 0.1 0.0 0.1 0.1

3.6 3.5 6.8 6.9 6.7

3.5 3.5 7.0 7.0 7.0

102.9

97.6 96.8 97.9

μg L -1 μg L -1 μg L -1

Adult Nutritional RTF High Protein Adult Nutritional RTF High Fat Infant Formula RTF, Milk-Based

102.9

Table D7: Data vitamin D 3

100% recovery experiment 1

(μg hg -1 )

Vitamin D 2

Recovery (%)

Sample

Units

Unspiked sample

Spiked sample

Spike

μg hg -1 μg hg -1

Child Formula Powder Infant Elemental Powder

0.0 0.0 0.0 0.0 0.0

10.4 10.0 20.0 21.1 20.2

7.2 7.2

100.2

96.1 96.7

μg L -1 μg L -1 μg L -1

Adult Nutritional RTF High Protein Adult Nutritional RTF High Fat Infant Formula RTF, Milk-Based

14.4 14.4 14.4

102.1

97.5

Table D8: Data vitamin D 3

50% recovery experiment 1

(μg hg -1 )

Vitamin D 2

Recovery (%)

Sample

Units

Unspiked sample

Spiked sample

Spike

μg hg -1 μg hg -1

Child Formula Powder Infant Elemental Powder

0.0 0.0 0.0 0.0 0.0

5.0 5.0

5.2 5.2

96.1 96.1 96.4 96.6 94.9

μg L -1 μg L -1 μg L -1

Adult Nutritional RTF High Protein Adult Nutritional RTF High Fat Infant Formula RTF, Milk-Based

10.0 10.0

10.3 10.3 10.3

9.8

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